Linked Life Data

16848496

Source:http://linkedlifedata.com/resource/pubmed/id/16848496

Statements in which the resource exists as a subject.
PredicateObject
rdf:type
lifeskim:mentions
pubmed:issue
15
pubmed:dateCreated
2006-7-19
pubmed:abstractText
In this paper, a method of determining trace levels of bromate in flour and related foods by ion chromatography with large volume injection has been proposed. The detection of bromate was performed with a suppressed conductivity detector after separation on an IonPac AS19 column with KOH as the gradient eluent. Parameters affecting the extraction efficiency of bromate, such as the flour-to-water ratio, extraction time, and temperature, were studied in detail. The optimized pretreatment process was then selected. By using the large volume injection technique, the solution detection limit was decreased to 0.5 microg/L. The linear range of this method was from 5 to 1000 microg/L, and the linear correlation coefficient was 0.9998. The method has been applied to the detection of bromate in flour and related foods, and different concentration levels of bromate were detected in various samples. The spiked recoveries ranged from 86 to 110%. The relative standard deviation (RSD) of the bromate peak height for the seven successive injections of the flour sample was 6.4%.
pubmed:language
eng
pubmed:journal
pubmed:citationSubset
IM
pubmed:chemical
pubmed:status
MEDLINE
pubmed:month
Jul
pubmed:issn
0021-8561
pubmed:author
pubmed:issnType
Print
pubmed:day
26
pubmed:volume
54
pubmed:owner
NLM
pubmed:authorsComplete
Y
pubmed:pagination
5217-9
pubmed:dateRevised
2006-11-15
pubmed:meshHeading
pubmed:year
2006
pubmed:articleTitle
Determination of trace levels of bromate in flour and related foods by ion chromatography.
pubmed:affiliation
State Key Laboratory of Environmental Chemistry and Ecotoxicity, Research Center for Eco-environmental Sciences, Chinese Academy of Sciences, Beijing 100085, China.
pubmed:publicationType
Journal Article, Research Support, Non-U.S. Gov't