Statements in which the resource exists as a subject.
PredicateObject
rdf:type
lifeskim:mentions
pubmed:issue
13
pubmed:dateCreated
2010-7-5
pubmed:abstractText
Seven food grade antioxidants were resolved by microemulsion electrokinetic chromatography. The antioxidants included propyl gallate, octyl gallate, dodecyl gallate, butylated hydroxyanisole, butylated hydroxytoluene, tert-butylhydroquinone and alpha-tocopherol. They were resolved in 11 min using a low pH microemulsion containing 20% propan-2-ol. Theoretical plates in the range 39,000-95,000 per length of column (38.5 cm) were recorded for the antioxidants. The LODs were calculated to be in the range 9-44 microg/mL (30 s hydrostatic injection and a 50 microm id capillary column). The method can also be used to simultaneously analyse for the synthetic preservatives sorbic acid, benzoic acid, salicylic acid and the parabens. The method was successfully applied to noodles for the determination of butylated hydroxytoluene and propyl gallate and to pharmaceutical supplement tablets for alpha-tocopherol. The in-capillary concentration of butylated hydroxytoluene by sweeping was also demonstrated.
pubmed:language
eng
pubmed:journal
pubmed:citationSubset
IM
pubmed:chemical
pubmed:status
MEDLINE
pubmed:month
Jul
pubmed:issn
1522-2683
pubmed:author
pubmed:issnType
Electronic
pubmed:volume
31
pubmed:owner
NLM
pubmed:authorsComplete
Y
pubmed:pagination
2267-71
pubmed:meshHeading
pubmed:year
2010
pubmed:articleTitle
Determination of food grade antioxidants using microemulsion electrokinetic chromatography.
pubmed:affiliation
School of Natural Sciences, Edith Cowan University, WA, Australia.
pubmed:publicationType
Journal Article