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Predicate | Object |
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rdf:type | |
lifeskim:mentions | |
pubmed:dateCreated |
1976-12-30
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pubmed:abstractText |
A quantitative method is described for determination of 4-heptanone and its precursor in urine. The method involves a single-step extraction of urine with cyclohexane and the analysis of 1 mul of the extract by gas chromatography-mass fragmentography. The detection limit is 8-10(-12)g, corresponding to 2 mug per 1000 ml of urine. The method is linear in the concentration range of 7.6-10(-9)-1.5-10(-5)g/ml and the relative standard deviations for the individual values are between 1.2 and 10%. Approximately 40 samples can be analyzed per day or 1 sample in 7-8 min. By varying the experimental conditions, the method is applicable to other ketones.
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pubmed:language |
eng
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pubmed:journal | |
pubmed:citationSubset |
IM
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pubmed:chemical | |
pubmed:status |
MEDLINE
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pubmed:month |
Nov
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pubmed:issn |
0021-9673
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pubmed:author | |
pubmed:issnType |
Print
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pubmed:day |
3
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pubmed:volume |
126
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pubmed:owner |
NLM
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pubmed:authorsComplete |
Y
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pubmed:pagination |
465-74
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pubmed:dateRevised |
2006-11-15
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pubmed:meshHeading |
pubmed-meshheading:977690-Chromatography, Gas,
pubmed-meshheading:977690-Cyclohexanes,
pubmed-meshheading:977690-Gas Chromatography-Mass Spectrometry,
pubmed-meshheading:977690-Humans,
pubmed-meshheading:977690-Ketones,
pubmed-meshheading:977690-Methods,
pubmed-meshheading:977690-Microchemistry,
pubmed-meshheading:977690-Molecular Weight,
pubmed-meshheading:977690-Time Factors
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pubmed:year |
1976
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pubmed:articleTitle |
Rapid quantitative microanalysis of ketones in urine by gas chromatography-mass fragmentography.
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pubmed:publicationType |
Journal Article
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