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| Predicate | Object |
|---|---|
| rdf:type | |
| lifeskim:mentions | |
| pubmed:issue |
1
|
| pubmed:dateCreated |
1984-4-24
|
| pubmed:abstractText |
A process was developed for production of gram quantities of deoxynivalenol (DON) from corn that had been inoculated in the field with Fusarium graminearum and was estimated to contain 400-500 mg DON/kg. Steps in the purification procedure included extraction with methanol-water (1 + 1), partition from an aqueous solution into ethyl acetate by using a hydrophilic matrix, defatting, Florisil column chromatography, methylene chloride-water partition, semipreparative liquid chromatography (LC), and crystallization from ethyl acetate. The average yield of crystalline DON produced by this method (or with minor variations) was 281 mg/kg.
|
| pubmed:language |
eng
|
| pubmed:journal | |
| pubmed:citationSubset |
IM
|
| pubmed:chemical | |
| pubmed:status |
MEDLINE
|
| pubmed:issn |
0004-5756
|
| pubmed:author | |
| pubmed:issnType |
Print
|
| pubmed:volume |
67
|
| pubmed:owner |
NLM
|
| pubmed:authorsComplete |
Y
|
| pubmed:pagination |
32-4
|
| pubmed:dateRevised |
2006-11-15
|
| pubmed:meshHeading |
pubmed-meshheading:6698925-Chromatography,
pubmed-meshheading:6698925-Chromatography, Liquid,
pubmed-meshheading:6698925-Crystallization,
pubmed-meshheading:6698925-Magnetic Resonance Spectroscopy,
pubmed-meshheading:6698925-Mass Spectrometry,
pubmed-meshheading:6698925-Sesquiterpenes,
pubmed-meshheading:6698925-Spectrophotometry, Infrared,
pubmed-meshheading:6698925-Trichothecenes,
pubmed-meshheading:6698925-Zea mays
|
| pubmed:articleTitle |
Preparation of deoxynivalenol (vomitoxin) from field-inoculated corn.
|
| pubmed:publicationType |
Journal Article
|