21487180

Source:http://linkedlifedata.com/resource/pubmed/id/21487180

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Predicate	Object
rdf:type	pubmed:Citation
lifeskim:mentions	umls-concept:C0006751, umls-concept:C0010424, umls-concept:C0040711, umls-concept:C0181061
pubmed:issue	Pt 3
pubmed:dateCreated	2011-4-13
pubmed:abstractText	Precise and convenient crystal reorientation is of experimental importance in macromolecular crystallography (MX). The development of multi-axis goniometers, such as the ESRF/EMBL mini-?, necessitates the corresponding development of calibration procedures that can be used for the setup, maintenance and troubleshooting of such devices. While traditional multi-axis goniometers require all rotation axes to intersect the unique point of the sample position, recently developed miniaturized instruments for sample reorientation in MX are not as restricted. However, the samples must always be re-centred following a change in orientation. To overcome this inconvenience and allow the use of multi-axis goniometers without the fundamental restriction of having all axes intersecting in the same point, an automatic translation correction protocol has been developed for such instruments. It requires precise information about the direction and location of the rotation axes. To measure and supply this information, a general, easy-to-perform translation calibration (TC) procedure has also been developed. The TC procedure is routinely performed on most MX beamlines at the ESRF and some results are presented for reference.
pubmed:commentsCorrections	http://linkedlifedata.com/resource/pubmed/commentcorrection/21487180-10531520, http://linkedlifedata.com/resource/pubmed/commentcorrection/21487180-10531527, http://linkedlifedata.com/resource/pubmed/commentcorrection/21487180-12832812, http://linkedlifedata.com/resource/pubmed/commentcorrection/21487180-17057338, http://linkedlifedata.com/resource/pubmed/commentcorrection/21487180-17587661, http://linkedlifedata.com/resource/pubmed/commentcorrection/21487180-18566507, http://linkedlifedata.com/resource/pubmed/commentcorrection/21487180-19171973, http://linkedlifedata.com/resource/pubmed/commentcorrection/21487180-1925561, http://linkedlifedata.com/resource/pubmed/commentcorrection/21487180-19844017, http://linkedlifedata.com/resource/pubmed/commentcorrection/21487180-19844027, http://linkedlifedata.com/resource/pubmed/commentcorrection/21487180-9757086
pubmed:language	eng
pubmed:journal	http://linkedlifedata.com/resource/pubmed/journal/8305825
pubmed:citationSubset	IM
pubmed:chemical	http://linkedlifedata.com/resource/pubmed/chemical/Macromolecular Substances
pubmed:status	MEDLINE
pubmed:month	May
pubmed:issn	1600-5724
pubmed:author	pubmed-author:BrockhauserSandorS, pubmed-author:McCarthyAndrew AAA, pubmed-author:RavelliRaimond B GRB, pubmed-author:WhiteKristopher IKI
pubmed:issnType	Electronic
pubmed:volume	67
pubmed:owner	NLM
pubmed:authorsComplete	Y
pubmed:pagination	219-28
pubmed:dateRevised	2011-7-28
pubmed:meshHeading	pubmed-meshheading:21487180-Calibration, pubmed-meshheading:21487180-Crystallography, pubmed-meshheading:21487180-Macromolecular Substances
pubmed:year	2011
pubmed:articleTitle	Translation calibration of inverse-kappa goniometers in macromolecular crystallography.
pubmed:affiliation	European Molecular Biology Laboratory, Grenoble, France. brockhauser@embl.fr
pubmed:publicationType	Journal Article, Research Support, Non-U.S. Gov't