Linked Life Data

20352851

Source:http://linkedlifedata.com/resource/pubmed/id/20352851

Statements in which the resource exists as a subject.
PredicateObject
rdf:type
lifeskim:mentions
pubmed:issue
1
pubmed:dateCreated
2010-3-31
pubmed:abstractText
Chalcopyrite, CuInSe2 was prepared by a fast microwave-assisted solvothermal synthesis. The influence of reaction temperature, concentrations of the constituents, types of copper salts and added solvent on the morphology and crystallinity of the chalcopyrite has been investigated and also the optimized parameters are presented. The optimum crystallinity was obtained at 180 degrees C reaction temperature with 0.02 M of copper ion concentration. Interestingly, when the copper acetate was used as a copper source, particle size of chalcopyrite was dramatically reduced. Moreover, the synthesis at 1L scale of the reactants gave the particle size of 20 nm for CuInSe2 which is smaller than that of small scale synthesis (23-35 nm). XRD, SEM and Raman Spectroscopy techniques are used for characterization and evaluation of the morphology of the chalcopyrite.
pubmed:language
eng
pubmed:journal
pubmed:status
PubMed-not-MEDLINE
pubmed:month
Jan
pubmed:issn
1533-4880
pubmed:author
pubmed:issnType
Print
pubmed:volume
10
pubmed:owner
NLM
pubmed:authorsComplete
Y
pubmed:pagination
303-8
pubmed:year
2010
pubmed:articleTitle
Microwave-assisted solvothermal synthesis of CuInSe2 chalcopyrites.
pubmed:affiliation
Research Center for Nanocatalysts, Korea Research Institute of Chemical Technology, Jang-dong 100, Yuseong, 305-600 Daejeon, South Korea.
pubmed:publicationType
Journal Article, Research Support, Non-U.S. Gov't