Source:http://linkedlifedata.com/resource/pubmed/id/20305725
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Predicate | Object |
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rdf:type | |
lifeskim:mentions | |
pubmed:issue |
9
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pubmed:dateCreated |
2010-4-1
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pubmed:abstractText |
Au nanocages synthesized from Ag nanocubes via the galvanic replacement reaction are finding widespread use in a range of applications because of their tunable optical properties. Most of these applications require the use of nanocages with a uniform size and in large quantities. This requirement translates into a demand for scaling up the production of Ag nanocubes with uniform, well-controlled sizes. Here we report such a method based on the modification of NaHS-mediated polyol synthesis with argon protection for fast reduction, which allows for the production of Ag nanocubes on a scale of 0.1 g per batch. The Ag nanocubes had an edge length tunable from 25 to 45 nm together with a size variation within +/-5 nm. The use of argon protection was the key to the success of this scale-up synthesis, suggesting the importance of controlling oxidative etching during synthesis.
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pubmed:grant | |
pubmed:language |
eng
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pubmed:journal | |
pubmed:citationSubset |
IM
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pubmed:chemical | |
pubmed:status |
MEDLINE
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pubmed:month |
Sep
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pubmed:issn |
1944-8244
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pubmed:author | |
pubmed:issnType |
Print
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pubmed:volume |
1
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pubmed:owner |
NLM
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pubmed:authorsComplete |
Y
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pubmed:pagination |
2044-8
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pubmed:dateRevised |
2011-9-26
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pubmed:meshHeading |
pubmed-meshheading:20305725-Argon,
pubmed-meshheading:20305725-Materials Testing,
pubmed-meshheading:20305725-Metal Nanoparticles,
pubmed-meshheading:20305725-Microscopy, Electron, Transmission,
pubmed-meshheading:20305725-Models, Chemical,
pubmed-meshheading:20305725-Nanostructures,
pubmed-meshheading:20305725-Nanotechnology,
pubmed-meshheading:20305725-Oxygen,
pubmed-meshheading:20305725-Polymers,
pubmed-meshheading:20305725-Silver,
pubmed-meshheading:20305725-Surface Plasmon Resonance,
pubmed-meshheading:20305725-Surface Properties
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pubmed:year |
2009
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pubmed:articleTitle |
Production of Ag nanocubes on a scale of 0.1 g per batch by protecting the NaHS-mediated polyol synthesis with argon.
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pubmed:affiliation |
Departments of Biomedical Engineering and of Chemistry, Washington University, St. Louis, Missouri 63130, USA.
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pubmed:publicationType |
Journal Article,
Research Support, Non-U.S. Gov't,
Research Support, N.I.H., Extramural
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