Source:http://linkedlifedata.com/resource/pubmed/id/19580978
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Predicate | Object |
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rdf:type | |
lifeskim:mentions | |
pubmed:issue |
2
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pubmed:dateCreated |
2009-7-28
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pubmed:abstractText |
Micrometer-sized mesoporous SBA-15 silica spheres have been synthesized using triblock copolymer poly(ethyleneoxide)-block-poly(propyleneoxide)-block-poly(ethyleneoxide) (EO(20)PO(70)EO(20)) as structure-directing agent with the assistance of 1,3,5-trimethylbenzene and KCl. By controlling the composition of synthesis gel, SBA-15 silica spheres with particle size in the range of 2-4.5 microm could be facilely obtained. The obtained SBA-15 silica spheres were characterized by X-ray diffraction, scanning electron microscopy, and N(2) physisorption technique. Dimethyloctadecylchlorosilane modified mesoporous SBA-15 silica with diameter of 4.5 microm was explored as stationary phase in high-performance liquid chromatography, and its chromatographic characteristics for separation of some small molecules and relatively large bio-molecules have been studied.
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pubmed:language |
eng
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pubmed:journal | |
pubmed:citationSubset |
IM
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pubmed:chemical | |
pubmed:status |
MEDLINE
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pubmed:month |
Sep
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pubmed:issn |
1095-7103
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pubmed:author | |
pubmed:issnType |
Electronic
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pubmed:day |
15
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pubmed:volume |
337
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pubmed:owner |
NLM
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pubmed:authorsComplete |
Y
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pubmed:pagination |
420-6
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pubmed:dateRevised |
2009-11-11
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pubmed:meshHeading |
pubmed-meshheading:19580978-Chromatography, High Pressure Liquid,
pubmed-meshheading:19580978-Microscopy, Electron, Scanning,
pubmed-meshheading:19580978-Particle Size,
pubmed-meshheading:19580978-Polyethylene Glycols,
pubmed-meshheading:19580978-Propylene Glycols,
pubmed-meshheading:19580978-Silicon Dioxide,
pubmed-meshheading:19580978-X-Ray Diffraction
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pubmed:year |
2009
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pubmed:articleTitle |
Facile synthesis of mesoporous SBA-15 silica spheres and its application for high-performance liquid chromatography.
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pubmed:affiliation |
Key Lab of Separation Science for Analytical Chemistry, Dalian Institute of Chemical Physics, Chinese Academy of Sciences, 457 Zhongshan Road, Dalian 116023, China.
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pubmed:publicationType |
Journal Article,
Research Support, Non-U.S. Gov't
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