Source:http://linkedlifedata.com/resource/pubmed/id/19353694
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rdf:type | |
lifeskim:mentions | |
pubmed:issue |
8
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pubmed:dateCreated |
2009-7-15
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pubmed:abstractText |
A method was developed and validated to quantify 3,4-dideoxyglucosone-3-ene in peritoneal dialysis fluids by high-performance liquid chromatography with UV detection after derivatization with o-phenylenediamine. The advantages of this method compared with direct HPLC analysis are (i) the possibility of quantifying 3,4-dideoxyglucosone-3-ene simultaneously together with other glucose degradation products, (ii) the compatibility of the method with MS detection for unequivocal identification of the analyte and (iii) a bathochromic shift of the UV absorbance maximum which leads to higher selectivity. The validated method was used to measure 3,4-dideoxyglucosone-3-ene concentrations additionally to the glucose degradation products 3-deoxyglucosone, methylglyoxal, glyoxal, 5-hydroxymethylfurfural, 2-furaldehyde, formaldehyde and acetaldehyde in 19 commercial products for peritoneal dialysis.
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pubmed:language |
eng
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pubmed:journal | |
pubmed:citationSubset |
IM
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pubmed:chemical |
http://linkedlifedata.com/resource/pubmed/chemical/1,2-diaminobenzene,
http://linkedlifedata.com/resource/pubmed/chemical/3,4-dideoxyglucosone-3-ene,
http://linkedlifedata.com/resource/pubmed/chemical/Dialysis Solutions,
http://linkedlifedata.com/resource/pubmed/chemical/Glucose,
http://linkedlifedata.com/resource/pubmed/chemical/Phenylenediamines,
http://linkedlifedata.com/resource/pubmed/chemical/Pyrones
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pubmed:status |
MEDLINE
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pubmed:month |
Aug
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pubmed:issn |
1099-0801
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pubmed:author | |
pubmed:copyrightInfo |
(c) 2009 John Wiley & Sons, Ltd.
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pubmed:issnType |
Electronic
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pubmed:volume |
23
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pubmed:owner |
NLM
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pubmed:authorsComplete |
Y
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pubmed:pagination |
843-51
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pubmed:meshHeading |
pubmed-meshheading:19353694-Chromatography, High Pressure Liquid,
pubmed-meshheading:19353694-Dialysis Solutions,
pubmed-meshheading:19353694-Glucose,
pubmed-meshheading:19353694-Humans,
pubmed-meshheading:19353694-Linear Models,
pubmed-meshheading:19353694-Peritoneal Dialysis,
pubmed-meshheading:19353694-Phenylenediamines,
pubmed-meshheading:19353694-Pyrones,
pubmed-meshheading:19353694-Sensitivity and Specificity
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pubmed:year |
2009
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pubmed:articleTitle |
Development and validation of an HPLC method to quantify 3,4-dideoxyglucosone-3-ene in peritoneal dialysis fluids.
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pubmed:affiliation |
Department of Chemistry and Pharmacy, Food Chemistry, University of Erlangen-Nuremberg, Erlangen, Germany.
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pubmed:publicationType |
Journal Article,
Validation Studies
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