rdf:type |
|
lifeskim:mentions |
umls-concept:C0008562,
umls-concept:C0018208,
umls-concept:C0043188,
umls-concept:C0220908,
umls-concept:C0392419,
umls-concept:C1171696,
umls-concept:C1172662,
umls-concept:C1510941,
umls-concept:C1511790,
umls-concept:C1613399,
umls-concept:C1707755
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pubmed:issue |
6
|
pubmed:dateCreated |
2005-7-15
|
pubmed:abstractText |
The Quinone outside Inhibitors (QoI) are one of the most important and recent fungicide groups used in viticulture and also allowed by Integrated Pest Management. Azoxystrobin, kresoxim-methyl and trifloxystrobin are the main active ingredients for treating downy and powdery mildews that can be present in grapes and wines. In this paper, a method is reported for the analysis of these three QoI-fungicides in grapes and wine. After liquid-liquid extraction and a clean-up on commercial silica cartridges, analysis was by isocratic HPLC with diode array detection (DAD) with a run time of 13 min. Confirmation was by solid-phase micro-extraction (SPME), followed by GC/MS determination. The main validation parameters for the three compounds in grapes and wine were a limit of detection up to 0.073 mg kg(-1), a precision not exceeding 10.0% and an average recovery of 93% +/- 38.
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pubmed:language |
eng
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pubmed:journal |
|
pubmed:citationSubset |
IM
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pubmed:chemical |
http://linkedlifedata.com/resource/pubmed/chemical/Acetates,
http://linkedlifedata.com/resource/pubmed/chemical/Acrylates,
http://linkedlifedata.com/resource/pubmed/chemical/Fungicides, Industrial,
http://linkedlifedata.com/resource/pubmed/chemical/Imines,
http://linkedlifedata.com/resource/pubmed/chemical/Methacrylates,
http://linkedlifedata.com/resource/pubmed/chemical/Pesticide Residues,
http://linkedlifedata.com/resource/pubmed/chemical/Phenylacetates,
http://linkedlifedata.com/resource/pubmed/chemical/Pyrimidines,
http://linkedlifedata.com/resource/pubmed/chemical/azoxystrobin,
http://linkedlifedata.com/resource/pubmed/chemical/kresoxim-methyl,
http://linkedlifedata.com/resource/pubmed/chemical/methyl...
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pubmed:status |
MEDLINE
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pubmed:month |
Jun
|
pubmed:issn |
0265-203X
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pubmed:author |
|
pubmed:issnType |
Print
|
pubmed:volume |
22
|
pubmed:owner |
NLM
|
pubmed:authorsComplete |
Y
|
pubmed:pagination |
549-56
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pubmed:dateRevised |
2006-11-15
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pubmed:meshHeading |
pubmed-meshheading:16019828-Acetates,
pubmed-meshheading:16019828-Acrylates,
pubmed-meshheading:16019828-Chromatography, High Pressure Liquid,
pubmed-meshheading:16019828-Food Analysis,
pubmed-meshheading:16019828-Food Contamination,
pubmed-meshheading:16019828-Fungicides, Industrial,
pubmed-meshheading:16019828-Imines,
pubmed-meshheading:16019828-Methacrylates,
pubmed-meshheading:16019828-Pesticide Residues,
pubmed-meshheading:16019828-Phenylacetates,
pubmed-meshheading:16019828-Pyrimidines,
pubmed-meshheading:16019828-Reproducibility of Results,
pubmed-meshheading:16019828-Vitis,
pubmed-meshheading:16019828-Wine
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pubmed:year |
2005
|
pubmed:articleTitle |
Screening of grapes and wine for azoxystrobin, kresoxim-methyl and trifloxystrobin fungicides by HPLC with diode array detection.
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pubmed:affiliation |
LEPAE-DEQ, Faculdade de Engenharia da Universidade do Porto, Portugal.
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pubmed:publicationType |
Journal Article,
Research Support, Non-U.S. Gov't,
Validation Studies
|