Linked Life Data

12238150

Source:http://linkedlifedata.com/resource/pubmed/id/12238150

Statements in which the resource exists as a subject.
PredicateObject
rdf:type
lifeskim:mentions
pubmed:issue
3
pubmed:dateCreated
2002-9-19
pubmed:abstractText
We investigated the determination of N-methylcarbamate pesticides and their metabolites in agricultural products by HPLC with post-column fluorescence detection after clean-up with an SPE cartridge. The homogenate of agricultural products was extracted with acetone. The crude extract was partitioned between 5% sodium chloride solution and dichloromethane, and the dichloromethane layer was concentrated to dryness. The residue was dissolved with a mixture of acetone and n-hexane, and purified by using Supelclean ENVI-Carb SPE, Bond Elut Extraction Cartridge PSA and SAX in series with a mixture of acetone and n-hexane. N-Methylcarbamate pesticide was analyzed by HPLC with post-column reaction and fluoresce detection. N-Methylcarbamate pesticide in citrus fruits and various kinds of agricultural products could be analyzed accurately by the presented method. Recoveries of N-methylcarbamate pesticides added to several agricultural products at the level of 0.10 ppm were mostly in the range of 60-110%. The limit of detection was 0.005 ppm.
pubmed:language
jpn
pubmed:journal
pubmed:citationSubset
IM
pubmed:chemical
pubmed:status
MEDLINE
pubmed:month
Jun
pubmed:issn
0015-6426
pubmed:author
pubmed:issnType
Print
pubmed:volume
43
pubmed:owner
NLM
pubmed:authorsComplete
Y
pubmed:pagination
133-43
pubmed:dateRevised
2006-11-15
pubmed:meshHeading
pubmed:year
2002
pubmed:articleTitle
[Simultaneous determination of N-methylcarbamate pesticides and their metabolites in agricultural products].
pubmed:affiliation
Tokyo Metropolitan Research Laboratory of Public Health: 3-24-1, Hyakunin-cho, Shinjuku-ku, Tokyo 169-0073, Japan.
pubmed:publicationType
Journal Article, English Abstract