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rdf:type |
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lifeskim:mentions |
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pubmed:issue |
17
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pubmed:dateCreated |
1999-2-1
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pubmed:abstractText |
A polymer-bound calcium sulfonate resin is prepared and used to sequester tetrabutylammonium fluoride. The simultaneous use of the calcium sulfonate resin with a sulfonic acid resin is used for the quenching and purification of desilylating reactions involving tetrabutylammonium fluoride as the reagent. Employment of this resin workup technique eliminates the need for a liquid-phase extractive protocol allowing the procedure to be easily automated.
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pubmed:language |
eng
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pubmed:journal |
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pubmed:citationSubset |
IM
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pubmed:chemical |
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pubmed:status |
MEDLINE
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pubmed:month |
Sep
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pubmed:issn |
0960-894X
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pubmed:author |
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pubmed:issnType |
Print
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pubmed:day |
8
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pubmed:volume |
8
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pubmed:owner |
NLM
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pubmed:authorsComplete |
Y
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pubmed:pagination |
2391-4
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pubmed:dateRevised |
2005-11-17
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pubmed:meshHeading |
pubmed-meshheading:9873547-Automation,
pubmed-meshheading:9873547-Chemistry, Organic,
pubmed-meshheading:9873547-Detergents,
pubmed-meshheading:9873547-Fluorides,
pubmed-meshheading:9873547-Indicators and Reagents,
pubmed-meshheading:9873547-Kinetics,
pubmed-meshheading:9873547-Molecular Conformation,
pubmed-meshheading:9873547-Molecular Structure,
pubmed-meshheading:9873547-Quaternary Ammonium Compounds,
pubmed-meshheading:9873547-Resins, Synthetic,
pubmed-meshheading:9873547-Silanes,
pubmed-meshheading:9873547-Structure-Activity Relationship
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pubmed:year |
1998
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pubmed:articleTitle |
A mixed resin bed for the quenching and purification of tetrabutylammonium fluoride mediated desilylating reactions.
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pubmed:affiliation |
Parallel Medicinal and Combinatorial Chemistry, Searle Discovery Research-U2D Monsanto Company, St. Louis, MO 63167, USA.
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pubmed:publicationType |
Journal Article
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