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Predicate | Object |
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rdf:type | |
lifeskim:mentions | |
pubmed:issue |
2
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pubmed:dateCreated |
1998-4-27
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pubmed:abstractText |
We propose a phase-sensitive gradient-enhanced two-dimensional heteronuclear multiple-bond correlation (psge-2D HMBC) experiment for speedy, accurate, and precise measurement of 2JCH and 3JCH. The experiment does not suppress one-bond correlations. Rather, the value of a desired long-range JCH is obtained from the pertinent cross-peak pattern in the HMBC spectrum, using the corresponding 1JCH correlation pattern as reference. The application of the proposed experiment is illustrated for the trisaccharide raffinose.
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pubmed:language |
eng
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pubmed:journal | |
pubmed:citationSubset |
IM
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pubmed:chemical | |
pubmed:status |
MEDLINE
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pubmed:month |
Feb
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pubmed:issn |
1090-7807
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pubmed:author | |
pubmed:copyrightInfo |
Copyright 1998 Academic Press.
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pubmed:issnType |
Print
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pubmed:volume |
130
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pubmed:owner |
NLM
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pubmed:authorsComplete |
Y
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pubmed:pagination |
296-9
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pubmed:dateRevised |
2006-11-15
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pubmed:meshHeading |
pubmed-meshheading:9500902-Fourier Analysis,
pubmed-meshheading:9500902-Image Processing, Computer-Assisted,
pubmed-meshheading:9500902-Magnetic Resonance Spectroscopy,
pubmed-meshheading:9500902-Molecular Structure,
pubmed-meshheading:9500902-Raffinose,
pubmed-meshheading:9500902-Reproducibility of Results,
pubmed-meshheading:9500902-Software
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pubmed:year |
1998
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pubmed:articleTitle |
Accurate and precise measurement of heteronuclear long-range couplings by a gradient-enhanced two-dimensional multiple-bond correlation experiment.
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pubmed:affiliation |
Department of Chemistry, Georgia State University, Atlanta, Georgia, 30303-3083, USA.
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pubmed:publicationType |
Journal Article,
Comparative Study
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