Linked Life Data

9468652

Source:http://linkedlifedata.com/resource/pubmed/id/9468652

Statements in which the resource exists as a subject.
PredicateObject
rdf:type
lifeskim:mentions
pubmed:issue
1
pubmed:dateCreated
1998-3-3
pubmed:abstractText
A simple and rapid isocratic HPLC assay is presented for the analysis and quantification of monoterpenes, i.e., carvone, cineole, perillaldehyde, perillyl alcohol and sobrerol in the diet of laboratory animals. The monoterpenes were extracted from the diet using 90% methanol in water. The analysis for the monoterpenes was performed by HPLC using a Whatman PartiSphere C18 column with UV detection. The mobile phase was isocratic methanol-water (72:28, v/v) for carvone, cineole, perillaldehyde and perillyl alcohol and methanol-water (65:35, v/v) for sobrerol. The method was simple with good repeatability (R.S.D. = 4.2-16.1%), reproducibility (R.S.D. = 3.7-19%), and accuracy (R.S.D. = 5.5-23.3%). The detection limit of the monoterpenes extracted from the diet was 2 micrograms/g for carvone, perillaldehyde and sobrerol, 20 micrograms/g for perillyl alcohol and 100 micrograms/g for cineole. Excellent resolution was achieved between the monoterpenes and the constituents of the diet. The method demonstrated applicability to monitoring the formulation of monoterpenes in the diet of laboratory animals.
pubmed:language
eng
pubmed:journal
pubmed:citationSubset
IM
pubmed:chemical
pubmed:status
MEDLINE
pubmed:month
Jan
pubmed:issn
0021-9673
pubmed:author
pubmed:issnType
Print
pubmed:day
9
pubmed:volume
793
pubmed:owner
NLM
pubmed:authorsComplete
Y
pubmed:pagination
71-6
pubmed:dateRevised
2009-1-15
pubmed:meshHeading
pubmed:year
1998
pubmed:articleTitle
Quantification of carvone, cineole, perillaldehyde, perillyl alcohol and sobrerol by isocratic high-performance liquid chromatography.
pubmed:affiliation
Department of Pathology, Medical College of Ohio, Toledo 43614, USA.
pubmed:publicationType
Journal Article, Comparative Study