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Predicate | Object |
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rdf:type | |
lifeskim:mentions | |
pubmed:issue |
2
|
pubmed:dateCreated |
1993-3-5
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pubmed:abstractText |
A sensitive and reliable method is described for the determination of aflatoxins B1, B2, G1 and G2, ochratoxin A and zearalenone in animal feed ingredients. A multi-toxin extraction and clean-up procedure is used, with dichloromethane-1 M hydrochloric acid (10:1) being used for the extraction and gel permeation chromatography being used for the clean-up. The liquid chromatographic method developed for the separation of the six mycotoxins involves gradient elution with a reversed-phase C18 column and fluorescence detection. Recoveries, repeatability and reproducibility have been determined on maize, palm and wheat. The detection limits varied depending on the type of feed.
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pubmed:language |
eng
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pubmed:journal | |
pubmed:citationSubset |
IM
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pubmed:chemical | |
pubmed:status |
MEDLINE
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pubmed:month |
Jan
|
pubmed:issn |
0021-9673
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pubmed:author | |
pubmed:issnType |
Print
|
pubmed:day |
22
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pubmed:volume |
629
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pubmed:owner |
NLM
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pubmed:authorsComplete |
Y
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pubmed:pagination |
229-35
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pubmed:dateRevised |
2006-11-15
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pubmed:meshHeading |
pubmed-meshheading:8429084-Aflatoxins,
pubmed-meshheading:8429084-Animal Feed,
pubmed-meshheading:8429084-Chromatography, Gel,
pubmed-meshheading:8429084-Chromatography, High Pressure Liquid,
pubmed-meshheading:8429084-Methylene Chloride,
pubmed-meshheading:8429084-Ochratoxins,
pubmed-meshheading:8429084-Plants,
pubmed-meshheading:8429084-Reproducibility of Results,
pubmed-meshheading:8429084-Triticum,
pubmed-meshheading:8429084-Zea mays,
pubmed-meshheading:8429084-Zearalenone
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pubmed:year |
1993
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pubmed:articleTitle |
Multimycotoxin detection and clean-up method for aflatoxins, ochratoxin and zearalenone in animal feed ingredients using high-performance liquid chromatography and gel permeation chromatography.
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pubmed:affiliation |
School of Chemical Sciences, Dublin City University, Glasnevin, Ireland.
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pubmed:publicationType |
Journal Article,
Research Support, Non-U.S. Gov't
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