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Predicate | Object |
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rdf:type | |
lifeskim:mentions | |
pubmed:dateCreated |
1986-9-16
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pubmed:abstractText |
A method is presented for the collection of dry fractions from a microbore high-performance liquid chromatographic column. These fractions are electrosprayed onto a foil strip that is being moved past the spray in steps. These solid deposits are in a form which is compatible with solid-phase secondary-ion mass spectrometry, in particular the time-of-flight instrument that has been developed in our laboratory. Because the type of ionization used in static secondary-ion spectrometry is essentially non-destructive, the non-volatile eluent is available for any other analytical method after mass analysis. The chromatogram of a mixture of peptides was re-constructed from the mass spectra of fractions collected in this way. This chromatogram is shown and its features are examined.
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pubmed:grant | |
pubmed:language |
eng
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pubmed:journal | |
pubmed:citationSubset |
IM
|
pubmed:chemical | |
pubmed:status |
MEDLINE
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pubmed:month |
May
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pubmed:issn |
0021-9673
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pubmed:author | |
pubmed:issnType |
Print
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pubmed:day |
30
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pubmed:volume |
359
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pubmed:owner |
NLM
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pubmed:authorsComplete |
Y
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pubmed:pagination |
489-97
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pubmed:dateRevised |
2007-11-14
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pubmed:meshHeading | |
pubmed:year |
1986
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pubmed:articleTitle |
Automated dry fraction collection for microbore high-performance liquid chromatography-mass spectrometry.
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pubmed:publicationType |
Journal Article,
Research Support, U.S. Gov't, P.H.S.,
Research Support, Non-U.S. Gov't
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