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Predicate | Object |
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rdf:type | |
lifeskim:mentions | |
pubmed:issue |
3
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pubmed:dateCreated |
1987-8-28
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pubmed:abstractText |
A spectrophotometric method for the determination of cyclamate was collaboratively studied in 9 laboratories. Ethyl acetate is added to extract cyclamate from acidic aqueous solution into water, and the cyclamate is then quantitatively converted to N,N-dichlorocyclohexylamine by adding excess hypochlorite. N,N-Dichlorocyclohexylamine is determined by measuring its UV absorption at 314 nm. Six samples, 3 soft drinks with cyclamate levels of 0.36-0.47 g/kg and 3 jams with levels of 1.23-1.50 g/kg, were included in the study. Average recoveries of cyclamate were 99.7% in the soft drinks and 103.8% in the jams. Reproducibility coefficients of variation were 6.7% for the soft drinks and 4.4% for the jams.
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pubmed:language |
eng
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pubmed:journal | |
pubmed:citationSubset |
IM
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pubmed:chemical | |
pubmed:status |
MEDLINE
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pubmed:issn |
0004-5756
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pubmed:author | |
pubmed:issnType |
Print
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pubmed:volume |
70
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pubmed:owner |
NLM
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pubmed:authorsComplete |
Y
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pubmed:pagination |
588-90
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pubmed:dateRevised |
2000-12-18
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pubmed:meshHeading |
pubmed-meshheading:3610976-Beverages,
pubmed-meshheading:3610976-Condiments,
pubmed-meshheading:3610976-Cyclamates,
pubmed-meshheading:3610976-Food Analysis,
pubmed-meshheading:3610976-Fruit,
pubmed-meshheading:3610976-Indicators and Reagents,
pubmed-meshheading:3610976-Spectrophotometry, Ultraviolet
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pubmed:articleTitle |
Spectrophotometric determination of cyclamate in foods: NMKL collaborative study.
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pubmed:publicationType |
Journal Article
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