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Predicate | Object |
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rdf:type | |
lifeskim:mentions | |
pubmed:issue |
5
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pubmed:dateCreated |
1987-6-26
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pubmed:abstractText |
Aqueous formaldehyde was stabilized in pH 7 phosphate buffer with excess sodium bisulfite of fixed and known concentration. The 5,5'-dithiobis(2-nitrobenzoic acid) (DTNB) procedure described previously was used to determine excess bisulfite colorimetrically. The slope of the calibration line (absorbance at 412 nm vs. formaldehyde concentration) is -0.350 A.U./ug CH2O/mL (correlation coefficient: 0.9995). The precision of the method at the 95% confidence level is indicated by the mean percentage relative error (1.81 +/- 1.67) and mean percentage standard error (0.42 +/- 0.39). Gaseous formaldehyde of known concentrations (ppm) in air was absorbed from air samples in pH 7 buffer and determined by the DTNB method. For the determination of formaldehyde in air, the precision and accuracy were demonstrated at the 95% confidence level by the mean percentage relative error (5.04 +/- 3.2), the mean percentage standard error (1.72 +/- 1.0), the mean percentage recovery (99.9 +/- 2.7), and the mean percentage absolute error (1.86 +/- 1.6). The graphic comparison of air concentration found vs. air concentration calculated shows a slope of 0.993 ppmfound/ppmcalcd (correlation coefficient: 0.9993).
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pubmed:language |
eng
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pubmed:journal | |
pubmed:citationSubset |
IM
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pubmed:chemical | |
pubmed:status |
MEDLINE
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pubmed:month |
May
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pubmed:issn |
0002-8894
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pubmed:author | |
pubmed:issnType |
Print
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pubmed:volume |
48
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pubmed:owner |
NLM
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pubmed:authorsComplete |
Y
|
pubmed:pagination |
420-4
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pubmed:dateRevised |
2006-11-15
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pubmed:meshHeading | |
pubmed:year |
1987
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pubmed:articleTitle |
Validation of a colorimetric method for determination of atmospheric formaldehyde.
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pubmed:publicationType |
Journal Article,
Comparative Study
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