Switch to
Predicate | Object |
---|---|
rdf:type | |
lifeskim:mentions | |
pubmed:issue |
2
|
pubmed:dateCreated |
1989-5-26
|
pubmed:abstractText |
An ion-exchange chromatographic method was developed to determine hypoglycin A (HG-A) levels in canned ackee fruit by using an amino acid analyzer. HG-A was extracted by homogenizing the sample in 80% alcohol. An isocratic buffer system, consisting of 30% sodium citrate buffer (pH 3.15) and 70% sodium chloride-sodium acetate buffer (pH 7.40) was used to obtain baseline separation between HG-A and the other amino acids. The system can detect HG-A levels as low as 4.8 micrograms/mL. HG-A levels in the edible portion of fruit in 6 cans ranged from 11.0 to 66.5 mg HG-A/can. Recoveries by standard addition averaged 102.5%.
|
pubmed:language |
eng
|
pubmed:journal | |
pubmed:citationSubset |
IM
|
pubmed:chemical | |
pubmed:status |
MEDLINE
|
pubmed:issn |
0004-5756
|
pubmed:author | |
pubmed:issnType |
Print
|
pubmed:volume |
72
|
pubmed:owner |
NLM
|
pubmed:authorsComplete |
Y
|
pubmed:pagination |
374-7
|
pubmed:dateRevised |
2001-3-23
|
pubmed:meshHeading |
pubmed-meshheading:2708289-Amino Acids,
pubmed-meshheading:2708289-Chromatography, Ion Exchange,
pubmed-meshheading:2708289-Cyclopropanes,
pubmed-meshheading:2708289-Food Preservation,
pubmed-meshheading:2708289-Fruit,
pubmed-meshheading:2708289-Hypoglycins,
pubmed-meshheading:2708289-Magnetic Resonance Spectroscopy
|
pubmed:articleTitle |
Ion-exchange chromatographic determination of hypoglycin A in canned ackee fruit.
|
pubmed:affiliation |
Food and Drug Administration, Atlanta, GA 30309.
|
pubmed:publicationType |
Journal Article
|