Statements in which the resource exists as a subject.
PredicateObject
rdf:type
pubmed:issue
Pt 11
pubmed:dateCreated
2011-5-17
pubmed:abstractText
The title compound, C(22)H(21)ClFNO(6), was synthesized by the 1,3-dipolar cyclo-addition reaction of dimethyl maleate, methyl 2-amino-2-phenyl-acetate and 2-chloro-4-fluoro-benzaldehyde. The pyrrolidine ring possesses an envelope conformation and the two benzene rings are oriented at a dihedral angle of 68.28?(7)°. Weak inter-molecular C-H?O hydrogen bonding is present in the crystal structure. One methyl group is disordered over two positions with a site-occupancy ratio of 0.651?(12):0.349?(12).
pubmed:commentsCorrections
pubmed:language
eng
pubmed:journal
pubmed:status
PubMed-not-MEDLINE
pubmed:issn
1600-5368
pubmed:author
pubmed:issnType
Electronic
pubmed:volume
65
pubmed:owner
NLM
pubmed:authorsComplete
Y
pubmed:pagination
o2927
pubmed:dateRevised
2011-11-11
pubmed:year
2009
pubmed:articleTitle
Trimethyl 5-(2-chloro-4-fluoro-phen-yl)-2-phenyl-pyrrolidine-2,3,4-tricarboxyl-ate.
pubmed:affiliation
College of Chemistry and Chemical Engineering, China West Normal University, Nanchong 637002, People's Republic of China.
pubmed:publicationType
Journal Article