rdf:type |
|
lifeskim:mentions |
|
pubmed:issue |
1
|
pubmed:dateCreated |
2010-11-24
|
pubmed:abstractText |
A new sample treatment method for the determination of four common booster biocides (Diuron, TCMTB, Irgarol 1051 and Dichlofluanid) in harbour sediment samples has been developed that uses liquid chromatography-tandem mass spectrometry (LC-MS/MS) after microwave-assisted extraction, followed by clean-up and a solid phase extraction preconcentration step (MAE-SPE). The effects of different variables on MAE-SPE were studied. The recoveries obtained were greater than 75%, and the relative standard deviation was less than 7%. The detection limits ranged between 0.1 and 0.3 ng g?¹. The developed methodology was successfully applied to the evaluation of the presence of booster biocides in sediment samples from different harbours and marinas of Gran Canaria Island (Canary Islands, Spain).
|
pubmed:language |
eng
|
pubmed:journal |
|
pubmed:citationSubset |
IM
|
pubmed:chemical |
http://linkedlifedata.com/resource/pubmed/chemical/2-(thiocyanomethylthio)benzothiazole,
http://linkedlifedata.com/resource/pubmed/chemical/Aniline Compounds,
http://linkedlifedata.com/resource/pubmed/chemical/Benzothiazoles,
http://linkedlifedata.com/resource/pubmed/chemical/Disinfectants,
http://linkedlifedata.com/resource/pubmed/chemical/Diuron,
http://linkedlifedata.com/resource/pubmed/chemical/Thiocyanates,
http://linkedlifedata.com/resource/pubmed/chemical/Triazines,
http://linkedlifedata.com/resource/pubmed/chemical/Water Pollutants, Chemical,
http://linkedlifedata.com/resource/pubmed/chemical/dichlofluanid,
http://linkedlifedata.com/resource/pubmed/chemical/irgarol 1051
|
pubmed:status |
MEDLINE
|
pubmed:month |
Jan
|
pubmed:issn |
1879-1298
|
pubmed:author |
|
pubmed:copyrightInfo |
Copyright © 2010 Elsevier Ltd. All rights reserved.
|
pubmed:issnType |
Electronic
|
pubmed:volume |
82
|
pubmed:owner |
NLM
|
pubmed:authorsComplete |
Y
|
pubmed:pagination |
96-102
|
pubmed:meshHeading |
pubmed-meshheading:20947123-Aniline Compounds,
pubmed-meshheading:20947123-Benzothiazoles,
pubmed-meshheading:20947123-Chromatography, Liquid,
pubmed-meshheading:20947123-Disinfectants,
pubmed-meshheading:20947123-Diuron,
pubmed-meshheading:20947123-Environmental Monitoring,
pubmed-meshheading:20947123-Geologic Sediments,
pubmed-meshheading:20947123-Microwaves,
pubmed-meshheading:20947123-Seawater,
pubmed-meshheading:20947123-Tandem Mass Spectrometry,
pubmed-meshheading:20947123-Thiocyanates,
pubmed-meshheading:20947123-Triazines,
pubmed-meshheading:20947123-Water Pollutants, Chemical
|
pubmed:year |
2011
|
pubmed:articleTitle |
Applicability of microwave-assisted extraction combined with LC-MS/MS in the evaluation of booster biocide levels in harbour sediments.
|
pubmed:affiliation |
Department of Chemistry, University of Las Palmas de Gran Canaria, Spain.
|
pubmed:publicationType |
Journal Article,
Research Support, Non-U.S. Gov't,
Evaluation Studies
|