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PredicateObject
rdf:type
lifeskim:mentions
pubmed:issue
1
pubmed:dateCreated
2010-5-11
pubmed:abstractText
In this work a downscaled multicommuted flow injection analysis setup for photometric determination is described. The setup consists of a flow system module and a LED based photometer, with a total internal volume of about 170 microL. The system was tested by developing an analytical procedure for the photometric determination of iodate in table salt using N,N-diethyl-henylenediamine (DPD) as the chromogenic reagent. Accuracy was accessed by applying the paired t-test between results obtained using the proposed procedure and a reference method, and no significant difference at the 95% confidence level was observed. Other profitable features, such as a low reagent consumption of 7.3 microg DPD per determination; a linear response ranging from 0.1 up to 3.0 m IO(3)(-), a relative standard deviation of 0.9% (n=11) for samples containing 0.5 m IO(3)(-), a detection limit of 17 microg L(-1) IO(3)(-), a sampling throughput of 117 determination per hour, and a waste generation 600 microL per determination, were also achieved.
pubmed:language
eng
pubmed:journal
pubmed:status
PubMed-not-MEDLINE
pubmed:month
May
pubmed:issn
1873-4324
pubmed:author
pubmed:copyrightInfo
Copyright 2010 Elsevier B.V. All rights reserved.
pubmed:issnType
Electronic
pubmed:day
23
pubmed:volume
668
pubmed:owner
NLM
pubmed:authorsComplete
Y
pubmed:pagination
3-7
pubmed:year
2010
pubmed:articleTitle
Downscaling a multicommuted flow injection analysis system for the photometric determination of iodate in table salt.
pubmed:affiliation
Universidade Federal do Recôncavo da Bahia, Centro de Ciências Exatas e Tecnológicas, Centro, Cruz das Almas, 44380-000, Bahia, Brazil.
pubmed:publicationType
Journal Article