Source:http://linkedlifedata.com/resource/pubmed/id/20457294
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rdf:type | |
lifeskim:mentions | |
pubmed:issue |
1
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pubmed:dateCreated |
2010-5-11
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pubmed:abstractText |
In this work a downscaled multicommuted flow injection analysis setup for photometric determination is described. The setup consists of a flow system module and a LED based photometer, with a total internal volume of about 170 microL. The system was tested by developing an analytical procedure for the photometric determination of iodate in table salt using N,N-diethyl-henylenediamine (DPD) as the chromogenic reagent. Accuracy was accessed by applying the paired t-test between results obtained using the proposed procedure and a reference method, and no significant difference at the 95% confidence level was observed. Other profitable features, such as a low reagent consumption of 7.3 microg DPD per determination; a linear response ranging from 0.1 up to 3.0 m IO(3)(-), a relative standard deviation of 0.9% (n=11) for samples containing 0.5 m IO(3)(-), a detection limit of 17 microg L(-1) IO(3)(-), a sampling throughput of 117 determination per hour, and a waste generation 600 microL per determination, were also achieved.
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pubmed:language |
eng
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pubmed:journal | |
pubmed:status |
PubMed-not-MEDLINE
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pubmed:month |
May
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pubmed:issn |
1873-4324
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pubmed:author | |
pubmed:copyrightInfo |
Copyright 2010 Elsevier B.V. All rights reserved.
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pubmed:issnType |
Electronic
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pubmed:day |
23
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pubmed:volume |
668
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pubmed:owner |
NLM
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pubmed:authorsComplete |
Y
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pubmed:pagination |
3-7
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pubmed:year |
2010
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pubmed:articleTitle |
Downscaling a multicommuted flow injection analysis system for the photometric determination of iodate in table salt.
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pubmed:affiliation |
Universidade Federal do Recôncavo da Bahia, Centro de Ciências Exatas e Tecnológicas, Centro, Cruz das Almas, 44380-000, Bahia, Brazil.
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pubmed:publicationType |
Journal Article
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