Source:http://linkedlifedata.com/resource/pubmed/id/20432099
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| Predicate | Object |
|---|---|
| rdf:type | |
| lifeskim:mentions | |
| pubmed:issue |
7
|
| pubmed:dateCreated |
2010-6-14
|
| pubmed:abstractText |
Trichlorfon is a thermally unstable insecticide that can be easily decomposed to dichlorvos at high temperatures. In this study, a liquid chromatography-tandem mass spectrometry (LC-MS/MS) method was developed for simultaneous determination of the residues of trichlorfon and dichlorvos in animal tissues. Trichlorfon and dichlorvos in animal tissues were extracted with dichloromethane, homogenized/shaken, concentrated, and determined by LC-MS/MS. The two insecticides can be effectively separated and individually determined. The limits of detection (LODs) of trichlorfon and dichlorvos were 0.04 and 0.07 microg kg(-1), respectively; the limits of quantification (LOQs) of the two insecticides were both 5 microg kg(-1). The average recoveries for three spiked blank samples at 10, 20 and 40 microg kg(-1) were in the range 85-106%, with relative standard deviations (RSDs) below 10.6%, which falls in a reasonable range for the analysis of the two insecticides in animal-derived foods. The method is fit-for-purpose for the simultaneous determination of residues of trichlorfon and dichlorvos in animal tissues.
|
| pubmed:language |
eng
|
| pubmed:journal | |
| pubmed:citationSubset |
IM
|
| pubmed:chemical | |
| pubmed:status |
MEDLINE
|
| pubmed:month |
Jul
|
| pubmed:issn |
1944-0057
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| pubmed:author | |
| pubmed:issnType |
Electronic
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| pubmed:volume |
27
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| pubmed:owner |
NLM
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| pubmed:authorsComplete |
Y
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| pubmed:pagination |
983-8
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| pubmed:meshHeading |
pubmed-meshheading:20432099-Analytic Sample Preparation Methods,
pubmed-meshheading:20432099-Animals,
pubmed-meshheading:20432099-Chromatography, High Pressure Liquid,
pubmed-meshheading:20432099-Dichlorvos,
pubmed-meshheading:20432099-Food Contamination,
pubmed-meshheading:20432099-Food Inspection,
pubmed-meshheading:20432099-Insecticides,
pubmed-meshheading:20432099-Limit of Detection,
pubmed-meshheading:20432099-Liver,
pubmed-meshheading:20432099-Meat,
pubmed-meshheading:20432099-Meat Products,
pubmed-meshheading:20432099-Muscle, Skeletal,
pubmed-meshheading:20432099-Pesticide Residues,
pubmed-meshheading:20432099-Reproducibility of Results,
pubmed-meshheading:20432099-Spectrometry, Mass, Electrospray Ionization,
pubmed-meshheading:20432099-Sus scrofa,
pubmed-meshheading:20432099-Tandem Mass Spectrometry,
pubmed-meshheading:20432099-Trichlorfon
|
| pubmed:year |
2010
|
| pubmed:articleTitle |
Simultaneous determination of residues of trichlorfon and dichlorvos in animal tissues by LC-MS/MS.
|
| pubmed:affiliation |
Key Laboratory of Biorheology Science and Technology Under Ministry of Education, College of Bioengineering, Chongqing University, Chongqing 400044, China.
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| pubmed:publicationType |
Journal Article,
Research Support, Non-U.S. Gov't,
Validation Studies
|