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PredicateObject
rdf:type
lifeskim:mentions
pubmed:issue
8
pubmed:dateCreated
2008-10-30
pubmed:abstractText
The analysis time for determination of boron in steel can be remarkably shortened by simultaneous distillation of methyl borate and evaporation of the distillate for analysis by ICP atomic-emission spectrometry. Methyl borate, distilled with a large quantity of methanol, is collected in 4% sodium hydroxide solution heated in a water-bath at 90 degrees. As the boiling point of the mixture of absorption solution and methanol is lower than 90 degrees, the solvent mixture is easily evaporated. The limit of detection corresponds to 35 ng of boron in 0.5 g of steel.
pubmed:language
eng
pubmed:journal
pubmed:status
PubMed-not-MEDLINE
pubmed:month
Aug
pubmed:issn
0039-9140
pubmed:author
pubmed:issnType
Print
pubmed:volume
33
pubmed:owner
NLM
pubmed:authorsComplete
Y
pubmed:pagination
691-3
pubmed:year
1986
pubmed:articleTitle
Rapid technique for distillation of methyl borate for ICP atomic-emission spectrometric determination of boron in steel.
pubmed:affiliation
The Research Institute for Iron, Steel and Other Metals, Tohoku University, Sendai 980, Japan.
pubmed:publicationType
Journal Article