Linked Life Data

18257313

Source:http://linkedlifedata.com/resource/pubmed/id/18257313

Statements in which the resource exists as a subject.
PredicateObject
rdf:type
lifeskim:mentions
pubmed:issue
6
pubmed:dateCreated
2008-2-8
pubmed:abstractText
A method was developed for the determination of azoxystrobin residues in fruits and vegetables by gas chromatography/mass spectrometry (GC/MS). Azoxystrobin residues were extracted with ethyl acetate-cyclohexane (1 : 1, v/v) by ultrasonication and then they were cleaned up on a silica solid-phase extraction (SPE) column to obtain an extract suitable for analysis by GC/MS in the selective ion monitoring (SIM) mode (the selected ion: m/z 344, 372, 388 and 403). The calibration curves were linear between area and concentration of azoxystrobin from 0.01 to 1.0 mg/kg with the correlation coefficient greater than 0.99. The average recoveries from spiked fruit and vegetable matrixes at three concentrations of 0.01, 0.1, 1.0 mg/kg ranged from 85.2% to 98.2% with relative standard deviation less than 21.5%. The limit of detection was 0.01 mg/kg and the limit of quantity was 0.05 mg/kg in fruit and vegetable matrixes, respectively.
pubmed:language
chi
pubmed:journal
pubmed:citationSubset
IM
pubmed:chemical
pubmed:status
MEDLINE
pubmed:month
Nov
pubmed:issn
1000-8713
pubmed:author
pubmed:issnType
Print
pubmed:volume
25
pubmed:owner
NLM
pubmed:authorsComplete
Y
pubmed:pagination
898-901
pubmed:meshHeading
pubmed:year
2007
pubmed:articleTitle
[Determination of azoxystrobin residues in fruits and vegetables by gas chromatography/mass spectrometry with solid-phase extraction].
pubmed:affiliation
Qinghai Entry-Exit Inspection and Quarantine Bureau, Xining 810000, China. bohb1212@163.com
pubmed:publicationType
Journal Article, English Abstract