Source:http://linkedlifedata.com/resource/pubmed/id/18207154
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Predicate | Object |
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rdf:type | |
lifeskim:mentions | |
pubmed:issue |
1-2
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pubmed:dateCreated |
2008-3-17
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pubmed:abstractText |
A simple and sensitive method for the determination of musty odorants, 2-methylisoborneol (MIB) and geosmin (GSM), in environmental water was developed by headspace solid-phase microextraction (HS-SPME) coupled with gas chromatography-mass spectrometry. MIB and GSM were separated within 10 min using a DB-1 capillary column and detected in the selective ion monitoring mode. HS-SPME using a polydimethylsiloxane/divinylbenzene fiber provided effective sample enrichment, and was carried out by fiber exposition at 70 degrees C for 30 min. Using this method, the calibration curves of MIB and GSM were linear in the range of 0-500 pg/mL, with a correlation coefficient above 0.9977 (n=24). The detection limits (S/N=3) of MIB and GSM were 0.9 and 0.6 pg/mL, respectively. This method was successfully applied to the analysis of environmental water samples without interference peaks.
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pubmed:language |
eng
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pubmed:journal | |
pubmed:citationSubset |
IM
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pubmed:chemical |
http://linkedlifedata.com/resource/pubmed/chemical/2-methylisoborneol,
http://linkedlifedata.com/resource/pubmed/chemical/Bornanes,
http://linkedlifedata.com/resource/pubmed/chemical/Naphthols,
http://linkedlifedata.com/resource/pubmed/chemical/Solutions,
http://linkedlifedata.com/resource/pubmed/chemical/Water,
http://linkedlifedata.com/resource/pubmed/chemical/geosmin
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pubmed:status |
MEDLINE
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pubmed:month |
Apr
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pubmed:issn |
0021-9673
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pubmed:author | |
pubmed:issnType |
Print
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pubmed:day |
4
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pubmed:volume |
1186
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pubmed:owner |
NLM
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pubmed:authorsComplete |
Y
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pubmed:pagination |
434-7
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pubmed:dateRevised |
2009-1-15
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pubmed:meshHeading |
pubmed-meshheading:18207154-Bornanes,
pubmed-meshheading:18207154-Calibration,
pubmed-meshheading:18207154-Environment,
pubmed-meshheading:18207154-Gas Chromatography-Mass Spectrometry,
pubmed-meshheading:18207154-Naphthols,
pubmed-meshheading:18207154-Odors,
pubmed-meshheading:18207154-Reference Standards,
pubmed-meshheading:18207154-Solid Phase Microextraction,
pubmed-meshheading:18207154-Solutions,
pubmed-meshheading:18207154-Temperature,
pubmed-meshheading:18207154-Time Factors,
pubmed-meshheading:18207154-Water
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pubmed:year |
2008
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pubmed:articleTitle |
Determination of musty odorants, 2-methylisoborneol and geosmin, in environmental water by headspace solid-phase microextraction and gas chromatography--mass spectrometry.
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pubmed:affiliation |
School of Pharmacy, Shujitsu University, Nishigawara, Okayama 703-8516, Japan.
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pubmed:publicationType |
Journal Article
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