Linked Life Data

18001100

Source:http://linkedlifedata.com/resource/pubmed/id/18001100

Statements in which the resource exists as a subject.
PredicateObject
rdf:type
lifeskim:mentions
pubmed:issue
26
pubmed:dateCreated
2007-12-14
pubmed:abstractText
Comparison is made between the preparation of trans-1,2-cyclohexanediol in standard glassware (conventional batch production) and in a microreactor (continuous flow production). The reaction sequence involved two exothermic steps where the standard procedure demands slow reagent addition and careful temperature control. In the microreactor, the reaction could be carried out safely with up to 3 times higher reagent concentration. Synthetic benefits were a faster reaction rate and a higher purity product free of colored impurities (a feature of the batch procedure).
pubmed:language
eng
pubmed:journal
pubmed:citationSubset
IM
pubmed:chemical
pubmed:status
MEDLINE
pubmed:month
Dec
pubmed:issn
0022-3263
pubmed:author
pubmed:issnType
Print
pubmed:day
21
pubmed:volume
72
pubmed:owner
NLM
pubmed:authorsComplete
Y
pubmed:pagination
10235-8
pubmed:meshHeading
pubmed:year
2007
pubmed:articleTitle
Advantages of synthesizing trans-1,2-cyclohexanediol in a continuous flow microreactor over a standard glass apparatus.
pubmed:affiliation
Chemistry and Chemical Engineering, School of Engineering & Physical Sciences, Heriot-Watt University, Riccarton, Edinburgh EH14 4AS, United Kingdom a.kraft@hw.ac.uk.
pubmed:publicationType
Journal Article, Research Support, Non-U.S. Gov't