rdf:type |
|
lifeskim:mentions |
|
pubmed:issue |
5
|
pubmed:dateCreated |
2007-10-5
|
pubmed:abstractText |
A rapid, simple and sensitive method was demonstrated for the determination of phenolic compounds in water samples by alternating-current oscillopolarographic titration. With the presence of sulfuric acid, phenol could be transferred into a nitroso-compound by reacting with NaNO2. The titration end-point was obtained by the formation of a sharp cut in the oscillopolarographic with infinitesimal NaNO2 on double platinum electrodes. The results showed that phenol concentration had an excellent linear relationship over the range of 4.82 x 10(-6)-9.65 x 10(-3) mol/L, the RSD of the proposed method was lower than 1.5%, and the spiked recoveries of three real water samples were in the range of 95.6%-106.9%.
|
pubmed:language |
eng
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pubmed:journal |
|
pubmed:citationSubset |
IM
|
pubmed:chemical |
|
pubmed:status |
MEDLINE
|
pubmed:issn |
1001-0742
|
pubmed:author |
|
pubmed:issnType |
Print
|
pubmed:volume |
19
|
pubmed:owner |
NLM
|
pubmed:authorsComplete |
Y
|
pubmed:pagination |
622-7
|
pubmed:dateRevised |
2008-2-8
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pubmed:meshHeading |
pubmed-meshheading:17915694-Bromides,
pubmed-meshheading:17915694-Electrochemistry,
pubmed-meshheading:17915694-Hydrogen-Ion Concentration,
pubmed-meshheading:17915694-Phenols,
pubmed-meshheading:17915694-Potassium Compounds,
pubmed-meshheading:17915694-Reproducibility of Results,
pubmed-meshheading:17915694-Sodium Nitrite,
pubmed-meshheading:17915694-Sulfuric Acids,
pubmed-meshheading:17915694-Temperature,
pubmed-meshheading:17915694-Titrimetry,
pubmed-meshheading:17915694-Water Pollutants, Chemical
|
pubmed:year |
2007
|
pubmed:articleTitle |
Rapid determination of phenolic compounds in water samples by alternating-current oscillopolarographic titration.
|
pubmed:affiliation |
Department of Chemistry, University of Science and Technology Beijing, Beijing 100083, China.
|
pubmed:publicationType |
Journal Article,
Research Support, Non-U.S. Gov't,
Evaluation Studies
|