Linked Life Data

17854817

Source:http://linkedlifedata.com/resource/pubmed/id/17854817

Statements in which the resource exists as a subject.
PredicateObject
rdf:type
lifeskim:mentions
pubmed:issue
2
pubmed:dateCreated
2007-9-24
pubmed:abstractText
A systematic study was made on the identification and quantitative determination of polynuclear aromatic hydrocarbons (PAHs) in heavy products derived from coal and petroleum with high performance liquid chromatography (HPLC). After the separation of PAHs by a high-resolution column, identification was made through four methods: (1) the relative retention time (RRT) method, (2) the stop-flow-UV scanning method, (3) the method of fluorescence characteristic index Phi' and (4) the method of V' index at different UV wavelengths. For the quantitative determination of the components, methods of external standard (E-X), internal standard (I-N) and external standard-response factors (E-F) were compared. The E-F method was recommended by the present paper. For the determination of quantitative response factors (F) two methods were studied, including the HPLC peak-area method (Peak-area method) and the UV absorbance method using a UV spectrometer (absorbance method). The absorbance method was better and is recommended by the present paper. The F values of 30 PAHs from the two different methods are given. The samples analyzed include a coal tar pitch, a thermal cracking residue oil and a residual oil from ethylene production.
pubmed:language
eng
pubmed:journal
pubmed:citationSubset
IM
pubmed:chemical
pubmed:status
MEDLINE
pubmed:month
Oct
pubmed:issn
0021-9673
pubmed:author
pubmed:issnType
Print
pubmed:day
12
pubmed:volume
1167
pubmed:owner
NLM
pubmed:authorsComplete
Y
pubmed:pagination
171-7
pubmed:dateRevised
2009-1-15
pubmed:meshHeading
pubmed:year
2007
pubmed:articleTitle
Analysis of polynuclear aromatic hydrocarbons in heavy products derived from coal and petroleum by high performance liquid chromatography.
pubmed:affiliation
State Key Laboratory of Coal Conversion, Institute of Coal Chemistry, Chinese Academy of Sciences, Taiyuan 030001, China. zhangcm@sxicc.ac.cn
pubmed:publicationType
Journal Article, Research Support, Non-U.S. Gov't