Linked Life Data

17723758

Source:http://linkedlifedata.com/resource/pubmed/id/17723758

Statements in which the resource exists as a subject.
PredicateObject
rdf:type
lifeskim:mentions
pubmed:issue
1
pubmed:dateCreated
2007-8-28
pubmed:abstractText
A rapid dynamic microwave-assisted extraction and on-line detection by spectrophotometry is proposed for the determination of safflower yellow in Flos Carthami. A high pressure and a peristaltic pump were used to deliver the solvent. A TM010 microwave resonance cavity was applied to concentrate the microwave energy and the forward power about 60 W was enough for the extraction. Other extraction conditions also were examined and optimized. In this work, the extraction process can be monitored by measuring the absorption of safflower yellow in the extract, which would be convenient for rapid optimization of the extraction process. The detection and quantification limits are 8 and 27 microg mL(-1), respectively. The within-day and between-day precision (R.S.D.) are 1.6-3.2% and 2.8-4.2%, respectively. Compared with off-line detection, the proposed method may provide more rapid measurement and is more convenient for obtaining continuous measurements.
pubmed:language
eng
pubmed:journal
pubmed:status
PubMed-not-MEDLINE
pubmed:month
Oct
pubmed:issn
1873-4324
pubmed:author
pubmed:issnType
Electronic
pubmed:day
27
pubmed:volume
580
pubmed:owner
NLM
pubmed:authorsComplete
Y
pubmed:pagination
75-82
pubmed:year
2006
pubmed:articleTitle
Dynamic microwave-assisted extraction coupled with on-line spectrophotometric determination of safflower yellow in Flos Carthami.
pubmed:affiliation
College of Chemistry, Jilin University, 2699 Qianjin Street, Changchun 130012, PR China.
pubmed:publicationType
Journal Article