Source:http://linkedlifedata.com/resource/pubmed/id/17300791
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Predicate | Object |
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rdf:type | |
lifeskim:mentions | |
pubmed:issue |
1-2
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pubmed:dateCreated |
2007-7-19
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pubmed:abstractText |
Last years, the usefulness of the use of carbon nanotubes (CNTs) as sorbent material have been demonstrated for a wide variety of compounds. In this work, it has been demonstrated for first time that immobilized carboxylated single-walled carbon nanotubes (c-SWNTs) offer clear advantages over the use of CNTs. The higher adsorption capacity has been attributed to the special orientation of c-SWNTs molecules on the glass surface. The potential of this new sorbent was evaluated for the preconcentration of non-steroidal anti-inflammatory drugs (NSAIDs) from urine samples. Purified samples were analysed by capillary electrophoresis-mass spectrometry detection allowing the determination of 1.6 to 2.6 microg/L of NSAIDs with only 5 mL of sample. The precision of the method for the determination of real spiked urine samples ranged from 5.4 to 7.4% and the recoveries from 98.6 to 102.2%.
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pubmed:language |
eng
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pubmed:journal | |
pubmed:citationSubset |
IM
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pubmed:chemical |
http://linkedlifedata.com/resource/pubmed/chemical/Anti-Inflammatory Agents...,
http://linkedlifedata.com/resource/pubmed/chemical/Carboxylic Acids,
http://linkedlifedata.com/resource/pubmed/chemical/Indomethacin,
http://linkedlifedata.com/resource/pubmed/chemical/Ketoprofen,
http://linkedlifedata.com/resource/pubmed/chemical/Methanol,
http://linkedlifedata.com/resource/pubmed/chemical/Nanotubes, Carbon,
http://linkedlifedata.com/resource/pubmed/chemical/Tolmetin
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pubmed:status |
MEDLINE
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pubmed:month |
Aug
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pubmed:issn |
0021-9673
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pubmed:author | |
pubmed:issnType |
Print
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pubmed:day |
3
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pubmed:volume |
1159
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pubmed:owner |
NLM
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pubmed:authorsComplete |
Y
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pubmed:pagination |
203-7
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pubmed:dateRevised |
2009-1-15
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pubmed:meshHeading |
pubmed-meshheading:17300791-Adsorption,
pubmed-meshheading:17300791-Anti-Inflammatory Agents, Non-Steroidal,
pubmed-meshheading:17300791-Carboxylic Acids,
pubmed-meshheading:17300791-Electrophoresis, Capillary,
pubmed-meshheading:17300791-Hydrogen-Ion Concentration,
pubmed-meshheading:17300791-Indomethacin,
pubmed-meshheading:17300791-Ketoprofen,
pubmed-meshheading:17300791-Methanol,
pubmed-meshheading:17300791-Nanotubes, Carbon,
pubmed-meshheading:17300791-Sensitivity and Specificity,
pubmed-meshheading:17300791-Solid Phase Extraction,
pubmed-meshheading:17300791-Spectrometry, Mass, Matrix-Assisted Laser...,
pubmed-meshheading:17300791-Tolmetin,
pubmed-meshheading:17300791-Urine
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pubmed:year |
2007
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pubmed:articleTitle |
Determination of non-steroidal anti-inflammatory drugs in urine by combining an immobilized carboxylated carbon nanotubes minicolumn for solid-phase extraction with capillary electrophoresis-mass spectrometry.
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pubmed:affiliation |
Department of Analytical Chemistry, Marie Curie Building (Annex), Campus de Rabanales, University of Cordoba, E-14071 Cordoba, Spain.
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pubmed:publicationType |
Journal Article,
Research Support, Non-U.S. Gov't
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