Source:http://linkedlifedata.com/resource/pubmed/id/16471519
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Predicate | Object |
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rdf:type | |
lifeskim:mentions | |
pubmed:issue |
1
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pubmed:dateCreated |
2006-2-13
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pubmed:abstractText |
We present a surfactant-assisted solvothermal approach for the controllable synthesis of a PbS nanocrystal at low temperature (85 degrees C). Nanotubes (400 nm in length with an outer diameter of 30 nm), bundle-like long nanorods (about 5-15 mum long and an average diameter of 100 nm), nanowires (5-20 mum in length and with a diameter of 20-50 nm), short nanorods (100-300 nm in length and an axial ratio of 5-10), nanoparticles (25 nm in width with an aspect ratio of 2), and nanocubes (a short axis length of 10 nm and a long axis length of 15 nm) were successfully prepared and characterized by transmission electron microscopy, scanning electron microscopy, and powder X-ray diffraction pattern. A series of experimental results indicated that several experimental factors, such as AOT concentration, ratio of [water]/[surfactant], reaction time, and ratio of the reagents, play key roles in the final morphologies of PbS. Possible formation mechanisms of PbS nanorods and nanotubes were proposed.
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pubmed:language |
eng
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pubmed:journal | |
pubmed:citationSubset |
IM
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pubmed:chemical |
http://linkedlifedata.com/resource/pubmed/chemical/Lead,
http://linkedlifedata.com/resource/pubmed/chemical/Sulfides,
http://linkedlifedata.com/resource/pubmed/chemical/Surface-Active Agents,
http://linkedlifedata.com/resource/pubmed/chemical/Water,
http://linkedlifedata.com/resource/pubmed/chemical/lead sulfide
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pubmed:status |
MEDLINE
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pubmed:month |
Jan
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pubmed:issn |
1520-6106
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pubmed:author | |
pubmed:issnType |
Print
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pubmed:day |
12
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pubmed:volume |
110
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pubmed:owner |
NLM
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pubmed:authorsComplete |
Y
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pubmed:pagination |
184-9
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pubmed:dateRevised |
2007-3-23
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pubmed:meshHeading |
pubmed-meshheading:16471519-Lead,
pubmed-meshheading:16471519-Nanostructures,
pubmed-meshheading:16471519-Particle Size,
pubmed-meshheading:16471519-Sulfides,
pubmed-meshheading:16471519-Surface Properties,
pubmed-meshheading:16471519-Surface-Active Agents,
pubmed-meshheading:16471519-Temperature,
pubmed-meshheading:16471519-Time Factors,
pubmed-meshheading:16471519-Water
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pubmed:year |
2006
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pubmed:articleTitle |
Synthesis and evolution of PbS nanocrystals through a surfactant-assisted solvothermal route.
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pubmed:affiliation |
Institute of Polyoxometalate Chemistry, Department of Chemistry, Northeast Normal University, Changchun 130024, P R China.
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pubmed:publicationType |
Journal Article,
Research Support, Non-U.S. Gov't
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