Source:http://linkedlifedata.com/resource/pubmed/id/15055406
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Predicate | Object |
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rdf:type | |
lifeskim:mentions | |
pubmed:issue |
3
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pubmed:dateCreated |
2004-4-1
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pubmed:abstractText |
A sensitive, specific, and reproducible capillary gas chromatography (GC) with micro-electron capture detection (micro-ECD) method using headspace solid-phase micro-extraction (HS-SPME) for the quantitative analysis of p,p'-DDE in rat whole blood and hair was developed. A 100 microm polydimethylsiloxane (PDMS) phase was used for the extraction. The obtained detection limits were 0.003 ng/mg and 0.004 ng/mg in whole blood and hair, respectively, at a signal-to-noise ratio of 3 (S/N = 3). Linearity was obtained in the ranges 0.003-2.0 ng/mg and 0.004-2.0 ng/mg in whole blood and hair, respectively, and the correlation coefficients of whole blood and hair were greater than 0.998. This method was successfully applied to the analysis of p,p'-DDE in rat whole blood and rat hair after an oral dose of p,p'-DDE.
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pubmed:language |
eng
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pubmed:journal | |
pubmed:citationSubset |
IM
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pubmed:chemical | |
pubmed:status |
MEDLINE
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pubmed:month |
Oct
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pubmed:issn |
0385-0005
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pubmed:author | |
pubmed:issnType |
Print
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pubmed:volume |
28
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pubmed:owner |
NLM
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pubmed:authorsComplete |
Y
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pubmed:pagination |
131-8
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pubmed:dateRevised |
2004-11-17
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pubmed:meshHeading |
pubmed-meshheading:15055406-Animals,
pubmed-meshheading:15055406-Blood,
pubmed-meshheading:15055406-Chromatography, Gas,
pubmed-meshheading:15055406-Dichlorodiphenyl Dichloroethylene,
pubmed-meshheading:15055406-Hair,
pubmed-meshheading:15055406-Insecticides,
pubmed-meshheading:15055406-Molecular Structure,
pubmed-meshheading:15055406-Rats,
pubmed-meshheading:15055406-Reproducibility of Results,
pubmed-meshheading:15055406-Sensitivity and Specificity,
pubmed-meshheading:15055406-Temperature
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pubmed:year |
2003
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pubmed:articleTitle |
Headspace solid-phase micro-extraction and gas chromatography with micro-electron capture detection for the measurement of p,p'-DDE in rat whole blood and hair.
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pubmed:affiliation |
Department of Forensic Medicine, Tokai University School of Medicine, Isehara, Kanagawa, Japan.
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pubmed:publicationType |
Journal Article
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