Linked Life Data

14733141

Source:http://linkedlifedata.com/resource/pubmed/id/14733141

Statements in which the resource exists as a subject.
PredicateObject
rdf:type
lifeskim:mentions
pubmed:issue
5
pubmed:dateCreated
2004-1-21
pubmed:abstractText
A simultaneous determination method of 7 N-methylcarbamate and 7 urea pesticides in agricultural products by liquid chromatography/mass spectrometry (LC/MS) has been developed. Under reversed-phase liquid chromatographic conditions, 14 pesticides were analyzed using electrospray ionization (ESI) with simultaneous acquisition of positive ions and negative ions. Fourteen pesticides were extracted with acetone, 10% NaCl solution was added, and the pesticides were re-extracted with dichloromethane. The extract was concentrated under reduced pressure, and dissolved in methanol. The detection limits of 14 pesticides ranged from 0.0012 to 0.0056 microgram/g. The recoveries of pesticides were from 36.5 to 112.5% [RSD (n = 3) ranged from 0.5 to 48.1%] for 4 agricultural products.
pubmed:language
jpn
pubmed:journal
pubmed:citationSubset
IM
pubmed:chemical
pubmed:status
MEDLINE
pubmed:month
Oct
pubmed:issn
0015-6426
pubmed:author
pubmed:issnType
Print
pubmed:volume
44
pubmed:owner
NLM
pubmed:authorsComplete
Y
pubmed:pagination
263-7
pubmed:dateRevised
2006-11-15
pubmed:meshHeading
pubmed:year
2003
pubmed:articleTitle
[Simultaneous determination of N-methylcarbamate and urea pesticides in agricultural products by LC/MS].
pubmed:affiliation
Kitakyushu City Institute of Environmental Sciences: 1-2-1, Shinike, Tobata-ku, Kitakyushu, Fukuoka 804-0082, Japan.
pubmed:publicationType
Journal Article, English Abstract