Source:http://linkedlifedata.com/resource/pubmed/id/12613825
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Predicate | Object |
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rdf:type | |
lifeskim:mentions | |
pubmed:issue |
1-2
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pubmed:dateCreated |
2003-3-4
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pubmed:abstractText |
A new high-performance liquid chromatography method is described for the simultaneous quantitation of amino acids and amines for 37 compounds (20 amino acids + 17 amines), as their o-phthaldialdehyde (OPA)-3-mercaptopropionic acid derivatives, within 53 min. Based on previously documented stoichiometric and reaction mechanism studies, derivatizations have been carried out with the OPA-SH-group = 1:50 containing reagents. Reliability and reproducibility of analyses have been considerably improved. Average reproducibility data in a wide concentration range of derivatives had RSD < or = 3.4%.
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pubmed:language |
eng
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pubmed:journal | |
pubmed:citationSubset |
IM
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pubmed:chemical |
http://linkedlifedata.com/resource/pubmed/chemical/Acetic Acid,
http://linkedlifedata.com/resource/pubmed/chemical/Amines,
http://linkedlifedata.com/resource/pubmed/chemical/Amino Acids,
http://linkedlifedata.com/resource/pubmed/chemical/Indicators and Reagents,
http://linkedlifedata.com/resource/pubmed/chemical/o-Phthalaldehyde
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pubmed:status |
MEDLINE
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pubmed:month |
Feb
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pubmed:issn |
0021-9673
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pubmed:author | |
pubmed:issnType |
Print
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pubmed:day |
14
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pubmed:volume |
987
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pubmed:owner |
NLM
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pubmed:authorsComplete |
Y
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pubmed:pagination |
311-22
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pubmed:dateRevised |
2009-1-15
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pubmed:meshHeading |
pubmed-meshheading:12613825-Acetic Acid,
pubmed-meshheading:12613825-Amines,
pubmed-meshheading:12613825-Amino Acids,
pubmed-meshheading:12613825-Beer,
pubmed-meshheading:12613825-Chromatography, High Pressure Liquid,
pubmed-meshheading:12613825-Indicators and Reagents,
pubmed-meshheading:12613825-Reproducibility of Results,
pubmed-meshheading:12613825-Spectrometry, Fluorescence,
pubmed-meshheading:12613825-Wine,
pubmed-meshheading:12613825-o-Phthalaldehyde
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pubmed:year |
2003
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pubmed:articleTitle |
New aspects of the simultaneous analysis of amino acids and amines as their o-phthaldialdehyde derivatives by high-performance liquid chromatography. Analysis of wine, beer and vinegar.
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pubmed:affiliation |
Institute of Inorganic and Analytical Chemistry, L. Eötvös University, P.O. Box 32, H-1518 Budapest 112, Hungary.
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pubmed:publicationType |
Journal Article,
Research Support, Non-U.S. Gov't
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