Linked Life Data

12541984

Source:http://linkedlifedata.com/resource/pubmed/id/12541984

Statements in which the resource exists as a subject.
PredicateObject
rdf:type
lifeskim:mentions
pubmed:issue
2
pubmed:dateCreated
2003-1-24
pubmed:abstractText
An efficient method with microchemical method and solid phase extraction (SPE) technique for the determination of oxadiazon residues in cereals by gas chromatography-mass spectrometry (GC-MS) has been established. The oxadiazon was extracted from the sample with benzene-hexane(1:1, V/V). The extract was cleaned-up by a column of 500 mg Supelclean LC-Alumina-N. When the blank rice and corn were spiked with oxadiazon in the range of 0.005 mg/kg-5.00 mg/kg, the recoveries were 90.4%-115.7% for rice and 81.3-109.7% for corn, and with RSD of 2%-6% and 4%-9% respectively. The limit of detection was 0.005 mg/kg. The method is rapid, sensitive, accurate and suitable for the analysis of pesticide residues.
pubmed:language
chi
pubmed:journal
pubmed:citationSubset
IM
pubmed:chemical
pubmed:status
MEDLINE
pubmed:month
Mar
pubmed:issn
1000-8713
pubmed:author
pubmed:issnType
Print
pubmed:volume
20
pubmed:owner
NLM
pubmed:authorsComplete
Y
pubmed:pagination
190-2
pubmed:dateRevised
2006-11-15
pubmed:meshHeading
pubmed:year
2002
pubmed:articleTitle
[Determination of oxadiazon residues in cereals by gas chromatography-mass spectrometry].
pubmed:affiliation
Hunan Entry-Exit Inspection and Quarantine Bureau, Changsha 410007, China. lyjhnciq@163.com
pubmed:publicationType
Journal Article, English Abstract