Source:http://linkedlifedata.com/resource/pubmed/id/12541847
Switch to
Predicate | Object |
---|---|
rdf:type | |
lifeskim:mentions | |
pubmed:issue |
1
|
pubmed:dateCreated |
2003-1-24
|
pubmed:abstractText |
A method for the determination of tiptolide in human plasma by gas chromatography-electron capture detection is described. An SE-54 capillary column (30 m x 0.25 mm i.d.) was used. Nitrogen was used as the carrier gas. After NaOH solution being added, the plasma was extracted with ether-chloroform (3:1, V/V) and then reacted with trifluoroacetic anhydride. A good linearity was obtained from 1.0 microgram/L to 50.0 micrograms/L of tiptolide in human plasma, r = 0.9990. The detection limit of it in plasma was 0.5 microgram/L. The average recovery was 96.3%. The method is sensitive and precise.
|
pubmed:language |
chi
|
pubmed:journal | |
pubmed:citationSubset |
IM
|
pubmed:chemical | |
pubmed:status |
MEDLINE
|
pubmed:month |
Jan
|
pubmed:issn |
1000-8713
|
pubmed:author | |
pubmed:issnType |
Print
|
pubmed:volume |
19
|
pubmed:owner |
NLM
|
pubmed:authorsComplete |
Y
|
pubmed:pagination |
58-9
|
pubmed:dateRevised |
2007-11-15
|
pubmed:meshHeading |
pubmed-meshheading:12541847-Chromatography, Gas,
pubmed-meshheading:12541847-Diterpenes,
pubmed-meshheading:12541847-Electrophoresis, Capillary,
pubmed-meshheading:12541847-Epoxy Compounds,
pubmed-meshheading:12541847-Humans,
pubmed-meshheading:12541847-Phenanthrenes,
pubmed-meshheading:12541847-Sensitivity and Specificity
|
pubmed:year |
2001
|
pubmed:articleTitle |
[Determination of triptolide in human plasma by gas chromatography-electron capture detection].
|
pubmed:affiliation |
Department of Clinical Pharmacology, Nanjing General Hospital of Nanjing Command PLA, Nanjing 210002, China. yllyj@elong.com
|
pubmed:publicationType |
Journal Article,
English Abstract
|