Source:http://linkedlifedata.com/resource/pubmed/id/11874332
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| Predicate | Object |
|---|---|
| rdf:type | |
| lifeskim:mentions | |
| pubmed:issue |
5
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| pubmed:dateCreated |
2002-3-4
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| pubmed:abstractText |
A new rigid angular bridging ligand, 7-oxa-dibenzofluorene-3,11-dicarboxylic acid (H(2)L), was synthesized by cyanation of known rac-6,6'-dibromo-1,1'-bi-2-naphthol followed by ring closure and hydrolysis with concentrated sulfuric acid and used for the self-assembly of nanoscopic molecular rectangle [Cu(4)(L)(4)(Py)(8)].2DMF.10H(2)O, 1, and 1-D coordination polymer [Co(2)(L)(2)(Py)(4)].2DMF.2H(2)O, 2. Both 1 and 2 contain open channels occupied by DMF and water guest molecules. Crystal data for 1:[?] triclinic, space group P(-)1, a = 8.869(2) A, b = 16.437(3) A, c = 21.586(4) A, alpha = 78.18(3), beta = 79.19(3), gamma = 83.66(3), U = 3017.0(11) A(3), and Z = 1. Crystal data for 2: triclinic, space group P(-)1, a = 8.254(2) A, b = 12.154(2) A, c = 15.348(3) A, alpha = 95.34(3), beta = 93.38(3), gamma = 94.37(3), U = 1525.1(5) A(3), and Z = 1.
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| pubmed:language |
eng
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| pubmed:journal | |
| pubmed:status |
PubMed-not-MEDLINE
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| pubmed:month |
Mar
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| pubmed:issn |
0020-1669
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| pubmed:author | |
| pubmed:issnType |
Print
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| pubmed:day |
11
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| pubmed:volume |
41
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| pubmed:owner |
NLM
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| pubmed:authorsComplete |
Y
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| pubmed:pagination |
1033-5
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| pubmed:dateRevised |
2003-11-3
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| pubmed:year |
2002
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| pubmed:articleTitle |
New rigid angular dicarboxylic acid for the construction of nanoscopic supramolecules: from a molecular rectangle to a 1-D coordination polymer.
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| pubmed:affiliation |
Department of Chemistry, CB#3290, University of North Carolina, Chapel Hill, NC 27599, USA.
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| pubmed:publicationType |
Journal Article
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