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pubmed-article:17386431pubmed:abstractTextA multiresidue HPLC method for identification and quantification of the synthetic acaricides fluvalinate, coumaphos, bromopropylate and its metabolite 4,4'-dibromobenzophenone in beeswax has been developed. Different techniques were tested and modified. The method consists of a sample preparation with isooctane followed by solid phase extraction using Florisil columns. Determination of the synthetic acaricides is achieved by HPLC with a photodiode array detector. Analytical performance of the proposed method, including sensitivity, accuracy and precision was satisfactory. The LOD for the analytes varied between 0.1 and 0.2 microg g(-1) wax and the recoveries between 70 and 110%. Relative standard deviation of the repeatability of the method is <15% and reproducibility is <31%.lld:pubmed
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pubmed-article:17386431pubmed:authorpubmed-author:LázaroReginaRlld:pubmed
pubmed-article:17386431pubmed:authorpubmed-author:Pérez-Arquill...lld:pubmed
pubmed-article:17386431pubmed:authorpubmed-author:AdamczykSabin...lld:pubmed
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pubmed-article:17386431pubmed:year2007lld:pubmed
pubmed-article:17386431pubmed:articleTitleDetermination of synthetic acaricides residues in beeswax by high-performance liquid chromatography with photodiode array detector.lld:pubmed
pubmed-article:17386431pubmed:affiliationDepartment of Animal Production and Food Science, Veterinary Faculty, University of Zaragoza, Miguel Servet 177, 50013 Zaragoza, Spain.lld:pubmed
pubmed-article:17386431pubmed:publicationTypeJournal Articlelld:pubmed
pubmed-article:17386431pubmed:publicationTypeResearch Support, Non-U.S. Gov'tlld:pubmed