| pubmed-article:16360666 | rdf:type | pubmed:Citation | lld:pubmed |
| pubmed-article:16360666 | lifeskim:mentions | umls-concept:C0001645 | lld:lifeskim |
| pubmed-article:16360666 | lifeskim:mentions | umls-concept:C0008555 | lld:lifeskim |
| pubmed-article:16360666 | lifeskim:mentions | umls-concept:C0205195 | lld:lifeskim |
| pubmed-article:16360666 | pubmed:issue | 1 | lld:pubmed |
| pubmed-article:16360666 | pubmed:dateCreated | 2006-1-9 | lld:pubmed |
| pubmed-article:16360666 | pubmed:abstractText | Solvent extractive two-phase menthoxycarbonyl (MnOC) derivatization was combined with trimethylsilyl (TMS) reaction for enantioseparation of beta-blockers by gas chromatography employing achiral DB-5 and DB-17 dual-columns of different polarity. beta-Blockers in alkaline solution were vortex-mixed with menthyl chloroformate present in dichloromethane to be extracted as diastereomeric N-MnOC derivatives. The subsequent O(N)-TMS reaction allowed complete enantioseparations of two beta-blockers and partial separations of five as N-MnOC/O(N)-TMS derivatives in a single analysis. The temperature-programmed retention index sets were characteristic of each derivative, facilitating chiral discrimination of each enantiomer. | lld:pubmed |
| pubmed-article:16360666 | pubmed:language | eng | lld:pubmed |
| pubmed-article:16360666 | pubmed:journal | http://linkedlifedata.com/r... | lld:pubmed |
| pubmed-article:16360666 | pubmed:citationSubset | IM | lld:pubmed |
| pubmed-article:16360666 | pubmed:chemical | http://linkedlifedata.com/r... | lld:pubmed |
| pubmed-article:16360666 | pubmed:chemical | http://linkedlifedata.com/r... | lld:pubmed |
| pubmed-article:16360666 | pubmed:chemical | http://linkedlifedata.com/r... | lld:pubmed |
| pubmed-article:16360666 | pubmed:chemical | http://linkedlifedata.com/r... | lld:pubmed |
| pubmed-article:16360666 | pubmed:status | MEDLINE | lld:pubmed |
| pubmed-article:16360666 | pubmed:month | Jan | lld:pubmed |
| pubmed-article:16360666 | pubmed:issn | 0021-9673 | lld:pubmed |
| pubmed-article:16360666 | pubmed:author | pubmed-author:KimKyoung-Rae... | lld:pubmed |
| pubmed-article:16360666 | pubmed:author | pubmed-author:PaikMan-Jeong... | lld:pubmed |
| pubmed-article:16360666 | pubmed:author | pubmed-author:NguyenDuc-Toa... | lld:pubmed |
| pubmed-article:16360666 | pubmed:issnType | Print | lld:pubmed |
| pubmed-article:16360666 | pubmed:day | 20 | lld:pubmed |
| pubmed-article:16360666 | pubmed:volume | 1103 | lld:pubmed |
| pubmed-article:16360666 | pubmed:owner | NLM | lld:pubmed |
| pubmed-article:16360666 | pubmed:authorsComplete | Y | lld:pubmed |
| pubmed-article:16360666 | pubmed:pagination | 177-81 | lld:pubmed |
| pubmed-article:16360666 | pubmed:dateRevised | 2009-1-15 | lld:pubmed |
| pubmed-article:16360666 | pubmed:meshHeading | pubmed-meshheading:16360666... | lld:pubmed |
| pubmed-article:16360666 | pubmed:meshHeading | pubmed-meshheading:16360666... | lld:pubmed |
| pubmed-article:16360666 | pubmed:meshHeading | pubmed-meshheading:16360666... | lld:pubmed |
| pubmed-article:16360666 | pubmed:meshHeading | pubmed-meshheading:16360666... | lld:pubmed |
| pubmed-article:16360666 | pubmed:meshHeading | pubmed-meshheading:16360666... | lld:pubmed |
| pubmed-article:16360666 | pubmed:year | 2006 | lld:pubmed |
| pubmed-article:16360666 | pubmed:articleTitle | N-Menthoxycarbonylation combined with trimethylsilylation for enantioseparation of beta-blockers by achiral dual-column gas chromatography. | lld:pubmed |
| pubmed-article:16360666 | pubmed:affiliation | Biometabolite Analysis Laboratory, College of Pharmacy, Sungkyunkwan University, Suwon 440-746, South Korea. | lld:pubmed |
| pubmed-article:16360666 | pubmed:publicationType | Journal Article | lld:pubmed |
