pubmed-article:18995862 | rdf:type | pubmed:Citation | lld:pubmed |
pubmed-article:18995862 | lifeskim:mentions | umls-concept:C0002520 | lld:lifeskim |
pubmed-article:18995862 | lifeskim:mentions | umls-concept:C0008555 | lld:lifeskim |
pubmed-article:18995862 | lifeskim:mentions | umls-concept:C0024868 | lld:lifeskim |
pubmed-article:18995862 | lifeskim:mentions | umls-concept:C0205195 | lld:lifeskim |
pubmed-article:18995862 | pubmed:issue | 1-2 | lld:pubmed |
pubmed-article:18995862 | pubmed:dateCreated | 2008-12-1 | lld:pubmed |
pubmed-article:18995862 | pubmed:abstractText | N-ethoxycarbonylation was combined with (S)-1-phenylethylamidation for enantioseparation of amino acids by gas chromatography (GC) and gas chromatography-mass spectrometry (GC-MS) on achiral capillary columns. The method provided complete enantioseparations of 12 amino acids as diastereomeric N-ethoxycarbonyl/(S)-1-phenylethylamides with exceptional resolutions for proline (R(s) > or = 9.9) and pipecolic acid (R(s) > or = 10.2). GC-MS analysis in selected ion monitoring mode employing standard addition method, facilitated quantitation of D-pipecolic acid in kidney bean (0.95 microg/10 mg) and adzuki bean (0.14 microg/10 mg). The peak area ratios indicated that they had the identical chiral composition at 2.5% for D-pipecolic acid and 97.5% for L-pipecolic acid. | lld:pubmed |
pubmed-article:18995862 | pubmed:language | eng | lld:pubmed |
pubmed-article:18995862 | pubmed:journal | http://linkedlifedata.com/r... | lld:pubmed |
pubmed-article:18995862 | pubmed:citationSubset | IM | lld:pubmed |
pubmed-article:18995862 | pubmed:chemical | http://linkedlifedata.com/r... | lld:pubmed |
pubmed-article:18995862 | pubmed:chemical | http://linkedlifedata.com/r... | lld:pubmed |
pubmed-article:18995862 | pubmed:chemical | http://linkedlifedata.com/r... | lld:pubmed |
pubmed-article:18995862 | pubmed:chemical | http://linkedlifedata.com/r... | lld:pubmed |
pubmed-article:18995862 | pubmed:status | MEDLINE | lld:pubmed |
pubmed-article:18995862 | pubmed:month | Dec | lld:pubmed |
pubmed-article:18995862 | pubmed:issn | 0021-9673 | lld:pubmed |
pubmed-article:18995862 | pubmed:author | pubmed-author:KimKyoung-Rae... | lld:pubmed |
pubmed-article:18995862 | pubmed:author | pubmed-author:LeeJinwooJ | lld:pubmed |
pubmed-article:18995862 | pubmed:author | pubmed-author:PaikMan-Jeong... | lld:pubmed |
pubmed-article:18995862 | pubmed:issnType | Print | lld:pubmed |
pubmed-article:18995862 | pubmed:day | 19 | lld:pubmed |
pubmed-article:18995862 | pubmed:volume | 1214 | lld:pubmed |
pubmed-article:18995862 | pubmed:owner | NLM | lld:pubmed |
pubmed-article:18995862 | pubmed:authorsComplete | Y | lld:pubmed |
pubmed-article:18995862 | pubmed:pagination | 151-6 | lld:pubmed |
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pubmed-article:18995862 | pubmed:year | 2008 | lld:pubmed |
pubmed-article:18995862 | pubmed:articleTitle | N-ethoxycarbonylation combined with (S)-1-phenylethylamidation for enantioseparation of amino acids by achiral gas chromatography and gas chromatography-mass spectrometry. | lld:pubmed |
pubmed-article:18995862 | pubmed:affiliation | Metabolomic Analysis Laboratory, Institute for Neuroregeneration and Stem Cell Research, School of Medicine, Ajou University, Suwon 443-721, South Korea. | lld:pubmed |
pubmed-article:18995862 | pubmed:publicationType | Journal Article | lld:pubmed |
pubmed-article:18995862 | pubmed:publicationType | Research Support, Non-U.S. Gov't | lld:pubmed |