Linked Life Data

18942782

Source:http://linkedlifedata.com/resource/pubmed/id/18942782

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pubmed-article:18942782pubmed:abstractTextDynamic nuclear polarization is combined with temperature-jump methods to develop a new 2D 13C-13C NMR experiment that yields a factor of 100-170 increase in sensitivity. The polaization step is performed at 100 K, and the sample is subsequently melted with a 10.6 microm laser pulse to yield a sample with highly polarized 13C spins. 13C detected 2D 13C-13C spectroscopy is performed in the usual manner.lld:pubmed
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pubmed-article:18942782pubmed:dateRevised2011-9-26lld:pubmed
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pubmed-article:18942782pubmed:articleTitleIn situ temperature-jump dynamic nuclear polarization: enhanced sensitivity in two dimensional 13C-13C correlation spectroscopy in solution.lld:pubmed
pubmed-article:18942782pubmed:affiliationFrancis Bitter Magnet Laboratory and Department of Chemistry, Massachusetts Institute of Technology, Cambridge, Massachusetts 02139, USA.lld:pubmed
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