Linked Life Data

17889842

Source:http://linkedlifedata.com/resource/pubmed/id/17889842

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SubjectPredicateObjectContext
pubmed-article:17889842rdf:typepubmed:Citationlld:pubmed
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pubmed-article:17889842pubmed:issue18lld:pubmed
pubmed-article:17889842pubmed:dateCreated2007-11-23lld:pubmed
pubmed-article:17889842pubmed:abstractTextMethyl alpha- and beta-D-glucopyranoside act as moderate chelators of a boron centre through their O-4/6 binding site whereas the trans/trans arrangement of the O-2/3/4 hydroxy functions is not suited to form a chelate with the small boron central atom. In this work we report the crystal structure of the bisdiolatoborate Na2[B(Me alpha-D-Glcp4,6H(-2))(Me alpha-D-Glcp3,4,6H(-3))].NaOH.8H2O (1) along with a combined 11B and 13C NMR spectroscopic studies of borate-pyranoside solutions at different concentrations and pH. It is shown that crystallisation of a bisdiolatoborate needs both a high pH and a high total concentration.lld:pubmed
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pubmed-article:17889842pubmed:authorpubmed-author:BennerKlausKlld:pubmed
pubmed-article:17889842pubmed:authorpubmed-author:KlüfersPeterPlld:pubmed
pubmed-article:17889842pubmed:authorpubmed-author:LabischOliver...lld:pubmed
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pubmed-article:17889842pubmed:year2007lld:pubmed
pubmed-article:17889842pubmed:articleTitleBorate esters of the methyl D-glucopyranosides.lld:pubmed
pubmed-article:17889842pubmed:affiliationDepartment of Chemistry and Biochemistry of the Ludwig Maximilian University Munich, Butenandtstr. 5-13, D-81377 Munich, Germany.lld:pubmed
pubmed-article:17889842pubmed:publicationTypeJournal Articlelld:pubmed
pubmed-article:17889842pubmed:publicationTypeResearch Support, Non-U.S. Gov'tlld:pubmed