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pubmed-article:17659871pubmed:abstractTextThe p38 mitogen-activated protein kinase inhibitor VX-745 is prepared rapidly and efficiently in a four-step sequence using a combination of conductive heating and microwave-mediated steps. Its inhibitory activity was confirmed in hTERT immortalized HCA2 and WS dermal fibroblasts at 0.5-1.0 microM concentration by ELISA and immunoblot assay, and displays excellent kinase selectivity over the related stress-activated kinase JNK.lld:pubmed
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pubmed-article:17659871pubmed:dateRevised2009-11-19lld:pubmed
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pubmed-article:17659871pubmed:articleTitleRapid synthesis of VX-745: p38 MAP kinase inhibition in Werner syndrome cells.lld:pubmed
pubmed-article:17659871pubmed:affiliationSchool of Chemistry, Main Building, Cardiff University, Park Place, Cardiff CF10 3AT, UK. Bagleymc@cardiff.ac.uklld:pubmed
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