| pubmed-article:14584699 | rdf:type | pubmed:Citation | lld:pubmed |
| pubmed-article:14584699 | lifeskim:mentions | umls-concept:C0337810 | lld:lifeskim |
| pubmed-article:14584699 | lifeskim:mentions | umls-concept:C0022262 | lld:lifeskim |
| pubmed-article:14584699 | lifeskim:mentions | umls-concept:C0079240 | lld:lifeskim |
| pubmed-article:14584699 | lifeskim:mentions | umls-concept:C1948027 | lld:lifeskim |
| pubmed-article:14584699 | lifeskim:mentions | umls-concept:C0024868 | lld:lifeskim |
| pubmed-article:14584699 | lifeskim:mentions | umls-concept:C0936012 | lld:lifeskim |
| pubmed-article:14584699 | lifeskim:mentions | umls-concept:C0392762 | lld:lifeskim |
| pubmed-article:14584699 | lifeskim:mentions | umls-concept:C0148405 | lld:lifeskim |
| pubmed-article:14584699 | pubmed:issue | 1-2 | lld:pubmed |
| pubmed-article:14584699 | pubmed:dateCreated | 2003-10-30 | lld:pubmed |
| pubmed-article:14584699 | pubmed:abstractText | A new method was developed for the determination of 2-furfural (2-F) and 5-methylfurfural (5-MF), two products of Maillard reaction in vinegar, with head-space solid-phase microextraction (HS-SPME) coupled to gas chromatography-mass spectrometry (GC-MS). A divinylbenzene (DVB)/carboxen (CAR)/polydimethylsiloxane (PDMS) fibre was used and SPME conditions were optimised, studying ionic strength effect, temperature effect and adsorption time. Both analytes were determined by calibration established on 2-furfural-d4 (2-F-d4). The method showed good linearity in the range studied (from 16 to 0.12 mg/l), with a regression coefficient r2 of 0.9999. Inter-batch precision and accuracy were found between 14.9 and 6.0% and between -11.7 and 0.2%, respectively. Detection limit was 15 microg/l. The method is simple and accurate and it has been applied to a series of balsamic and non-balsamic vinegars. | lld:pubmed |
| pubmed-article:14584699 | pubmed:language | eng | lld:pubmed |
| pubmed-article:14584699 | pubmed:journal | http://linkedlifedata.com/r... | lld:pubmed |
| pubmed-article:14584699 | pubmed:citationSubset | IM | lld:pubmed |
| pubmed-article:14584699 | pubmed:chemical | http://linkedlifedata.com/r... | lld:pubmed |
| pubmed-article:14584699 | pubmed:chemical | http://linkedlifedata.com/r... | lld:pubmed |
| pubmed-article:14584699 | pubmed:chemical | http://linkedlifedata.com/r... | lld:pubmed |
| pubmed-article:14584699 | pubmed:chemical | http://linkedlifedata.com/r... | lld:pubmed |
| pubmed-article:14584699 | pubmed:chemical | http://linkedlifedata.com/r... | lld:pubmed |
| pubmed-article:14584699 | pubmed:status | MEDLINE | lld:pubmed |
| pubmed-article:14584699 | pubmed:month | Oct | lld:pubmed |
| pubmed-article:14584699 | pubmed:issn | 0021-9673 | lld:pubmed |
| pubmed-article:14584699 | pubmed:author | pubmed-author:RotilioDomeni... | lld:pubmed |
| pubmed-article:14584699 | pubmed:author | pubmed-author:GiordanoLucia... | lld:pubmed |
| pubmed-article:14584699 | pubmed:author | pubmed-author:CalabreseRobe... | lld:pubmed |
| pubmed-article:14584699 | pubmed:author | pubmed-author:DavoliEnricoE | lld:pubmed |
| pubmed-article:14584699 | pubmed:issnType | Print | lld:pubmed |
| pubmed-article:14584699 | pubmed:day | 31 | lld:pubmed |
| pubmed-article:14584699 | pubmed:volume | 1017 | lld:pubmed |
| pubmed-article:14584699 | pubmed:owner | NLM | lld:pubmed |
| pubmed-article:14584699 | pubmed:authorsComplete | Y | lld:pubmed |
| pubmed-article:14584699 | pubmed:pagination | 141-9 | lld:pubmed |
| pubmed-article:14584699 | pubmed:dateRevised | 2009-1-15 | lld:pubmed |
| pubmed-article:14584699 | pubmed:meshHeading | pubmed-meshheading:14584699... | lld:pubmed |
| pubmed-article:14584699 | pubmed:meshHeading | pubmed-meshheading:14584699... | lld:pubmed |
| pubmed-article:14584699 | pubmed:meshHeading | pubmed-meshheading:14584699... | lld:pubmed |
| pubmed-article:14584699 | pubmed:meshHeading | pubmed-meshheading:14584699... | lld:pubmed |
| pubmed-article:14584699 | pubmed:meshHeading | pubmed-meshheading:14584699... | lld:pubmed |
| pubmed-article:14584699 | pubmed:meshHeading | pubmed-meshheading:14584699... | lld:pubmed |
| pubmed-article:14584699 | pubmed:meshHeading | pubmed-meshheading:14584699... | lld:pubmed |
| pubmed-article:14584699 | pubmed:year | 2003 | lld:pubmed |
| pubmed-article:14584699 | pubmed:articleTitle | Quantitative analysis of 2-furfural and 5-methylfurfural in different Italian vinegars by headspace solid-phase microextraction coupled to gas chromatography-mass spectrometry using isotope dilution. | lld:pubmed |
| pubmed-article:14584699 | pubmed:affiliation | Gennaro Paone Environmental Health Center, Mario Negri Institute for Pharmacological Research, Consorzio Mario Negri Sud, Via Nazionale, 66030 Santa Maria Imbaro, Chieti, Italy. | lld:pubmed |
| pubmed-article:14584699 | pubmed:publicationType | Journal Article | lld:pubmed |
| pubmed-article:14584699 | pubmed:publicationType | Research Support, Non-U.S. Gov't | lld:pubmed |
